Structural characteristics of 2-halo-1,3,2-dithiarsenic compounds and tris-(pentafluorophenylthio)-arsen
Publication type: Journal Article
Publication date: 2006-04-01
scimago Q3
wos Q2
SJR: 0.385
CiteScore: 4.1
Impact factor: 2.4
ISSN: 0022328X, 18728561
Materials Chemistry
Organic Chemistry
Biochemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
The combination of various dithiols and AsX3 (X = F, Cl) produces the series of cyclized halo-arsenic dithiolate compounds: 2-chloro-1,3,2-dithiarsolane [AsCl(SCH2CH2S)] (1), 2-iodo-1,3,2-dithiarsolane [AsI(SCH2CH2S)] (2), 2-chloro-1,3,2-dithiarsenane [AsCl(SCH2CH2CH2S)] (3), 2-iodo-1,3,2-dithiarsenane [AsI(SCH2CH2CH2S)] (4), 3-chloro-4H,7H-5,6-benz-1,3,2-dithiarsepine [AsCl(SCH2)2(C6H4)] (5), 1,2-bis-dithiarsolan-2-ylmercapto-ethane [As2(SCH2CH2S)2(SCH2CH2S)] (6) and tris-(pentafluorophenylthio)-arsen [As(SC6F5)3] (7). The geometry around As for these compounds is best described as trigonal pyramidal with varying degrees of distortion. Compound 1 crystallizes in two polymorphic forms with similar structural parameters. The compounds have been characterized by IR, 1H, 19F, and 13C NMR, X-ray crystallography and GC–MS.
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Shaikh T. A. et al. Structural characteristics of 2-halo-1,3,2-dithiarsenic compounds and tris-(pentafluorophenylthio)-arsen // Journal of Organometallic Chemistry. 2006. Vol. 691. No. 9. pp. 1825-1833.
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Shaikh T. A., Bakus R. C., Parkin S., Atwood D. A. Structural characteristics of 2-halo-1,3,2-dithiarsenic compounds and tris-(pentafluorophenylthio)-arsen // Journal of Organometallic Chemistry. 2006. Vol. 691. No. 9. pp. 1825-1833.
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TY - JOUR
DO - 10.1016/j.jorganchem.2005.12.034
UR - https://doi.org/10.1016/j.jorganchem.2005.12.034
TI - Structural characteristics of 2-halo-1,3,2-dithiarsenic compounds and tris-(pentafluorophenylthio)-arsen
T2 - Journal of Organometallic Chemistry
AU - Shaikh, Taimur A
AU - Bakus, Ronald C
AU - Parkin, Sean
AU - Atwood, David A
PY - 2006
DA - 2006/04/01
PB - Elsevier
SP - 1825-1833
IS - 9
VL - 691
SN - 0022-328X
SN - 1872-8561
ER -
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@article{2006_Shaikh,
author = {Taimur A Shaikh and Ronald C Bakus and Sean Parkin and David A Atwood},
title = {Structural characteristics of 2-halo-1,3,2-dithiarsenic compounds and tris-(pentafluorophenylthio)-arsen},
journal = {Journal of Organometallic Chemistry},
year = {2006},
volume = {691},
publisher = {Elsevier},
month = {apr},
url = {https://doi.org/10.1016/j.jorganchem.2005.12.034},
number = {9},
pages = {1825--1833},
doi = {10.1016/j.jorganchem.2005.12.034}
}
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MLA
Copy
Shaikh, Taimur A., et al. “Structural characteristics of 2-halo-1,3,2-dithiarsenic compounds and tris-(pentafluorophenylthio)-arsen.” Journal of Organometallic Chemistry, vol. 691, no. 9, Apr. 2006, pp. 1825-1833. https://doi.org/10.1016/j.jorganchem.2005.12.034.