A Study of 2,3,4,5-tetrakis(2-thienyl)-1-monophosphole and 2,3,4,5-tetrakis(2-thienyl)-1-monophosphaferrocene as building blocks for π-conjugated systems
Almaz A Zagidullin
1, 2
,
Alena R. Lakomkina
1, 3
,
Anastasiia P. Samorodnova
1, 3
,
Mikhail Khrizanforov
1, 3
,
Ilya A Bezkishko
1
,
Publication type: Journal Article
Publication date: 2024-06-01
scimago Q3
wos Q2
SJR: 0.385
CiteScore: 4.1
Impact factor: 2.4
ISSN: 0022328X, 18728561
Abstract
The synthesis of tetraaryl-substituted 1-monophospholes and 1-monophosphaferrocenes, bearing 4-bromophenyl and 2-thienyl substituents at the PCα carbon atoms are described. It was shown that the reaction of n-octyl chloride with a mixture of sodium 1,2,3-tri- and 1-monophospholides results in the exclusive formation of new luminescent 1-n-octyl-1-monophospholes. All novel compounds have been fully characterized by NMR spectroscopy and mass-spectrometry, their optical and electrochemical behaviors have been elucidated. Phosphaferrocene-based compounds exhibit higher oxidation stability and higher HOMO-LUMO separation compared to the corresponding 1-monophosphole units.
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Zagidullin A. A. et al. A Study of 2,3,4,5-tetrakis(2-thienyl)-1-monophosphole and 2,3,4,5-tetrakis(2-thienyl)-1-monophosphaferrocene as building blocks for π-conjugated systems // Journal of Organometallic Chemistry. 2024. Vol. 1013. p. 123163.
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Zagidullin A. A., Lakomkina A. R., Gerasimova T. I., Samorodnova A. P., Khrizanforov M., Bezkishko I. A., Miluykov V. A Study of 2,3,4,5-tetrakis(2-thienyl)-1-monophosphole and 2,3,4,5-tetrakis(2-thienyl)-1-monophosphaferrocene as building blocks for π-conjugated systems // Journal of Organometallic Chemistry. 2024. Vol. 1013. p. 123163.
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TY - JOUR
DO - 10.1016/j.jorganchem.2024.123163
UR - https://linkinghub.elsevier.com/retrieve/pii/S0022328X2400158X
TI - A Study of 2,3,4,5-tetrakis(2-thienyl)-1-monophosphole and 2,3,4,5-tetrakis(2-thienyl)-1-monophosphaferrocene as building blocks for π-conjugated systems
T2 - Journal of Organometallic Chemistry
AU - Zagidullin, Almaz A
AU - Lakomkina, Alena R.
AU - Gerasimova, Tatiana I.
AU - Samorodnova, Anastasiia P.
AU - Khrizanforov, Mikhail
AU - Bezkishko, Ilya A
AU - Miluykov, Vasili
PY - 2024
DA - 2024/06/01
PB - Elsevier
SP - 123163
VL - 1013
SN - 0022-328X
SN - 1872-8561
ER -
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@article{2024_Zagidullin,
author = {Almaz A Zagidullin and Alena R. Lakomkina and Tatiana I. Gerasimova and Anastasiia P. Samorodnova and Mikhail Khrizanforov and Ilya A Bezkishko and Vasili Miluykov},
title = {A Study of 2,3,4,5-tetrakis(2-thienyl)-1-monophosphole and 2,3,4,5-tetrakis(2-thienyl)-1-monophosphaferrocene as building blocks for π-conjugated systems},
journal = {Journal of Organometallic Chemistry},
year = {2024},
volume = {1013},
publisher = {Elsevier},
month = {jun},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0022328X2400158X},
pages = {123163},
doi = {10.1016/j.jorganchem.2024.123163}
}