Elsevier
Journal of Pharmaceutical and Biomedical Analysis
,  том 41 ,  издание 4 ,  страницы 1418-1422

Characterization of related impurities in megestrol acetate

Тип публикации: Journal Article
Дата публикации: 2006-06-01
Elsevier
scimago Q2
wos Q2
БС1
SJR: 0.628
CiteScore: 6.4
Impact factor: 3.1
ISSN: 07317085, 1873264X
Drug Discovery
Spectroscopy
Pharmaceutical Science
Clinical Biochemistry
Analytical Chemistry
Краткое описание
Three new compounds, 17alpha-acetoxy-2,6-dimethylpregna-1,4,6-triene-3,20-dione (1), 17alpha-acetoxy-2alpha,6-dimethylpregna-4,6-diene-3,20-dione (2), 17alpha-acetoxy-6alpha-methoxylmethylpregna-4-ene-3,20-dione (3), together with five known ones, 17alpha-acetoxy-6beta-hydroxyl-6alpha-methylpregna-4-ene-3,20-dione (4), 17alpha-acetoxy-6alpha-hydroxyl-6beta-methylpregna-4-ene-3,20-dione (5), 17alpha-acetoxy-pregna-4-ene-3,6,20-trione (6), 17alpha-acetoxy-pregna-4-ene-3,20-dione (7) and 17alpha-acetoxy-6-methylene-pregna-4-ene-3,20-dione (8), were isolated and identified from the residual mother liquor of megestrol acetate. Their structures were established by spectroscopic methods. These compounds seem to be minor impurities in production of the drug megestrol acetate.
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Guo F. et al. Characterization of related impurities in megestrol acetate // Journal of Pharmaceutical and Biomedical Analysis. 2006. Vol. 41. No. 4. pp. 1418-1422.
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Guo F., Feng H., Wang Y., Zhang C., Li Y. Characterization of related impurities in megestrol acetate // Journal of Pharmaceutical and Biomedical Analysis. 2006. Vol. 41. No. 4. pp. 1418-1422.
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TY - JOUR
DO - 10.1016/j.jpba.2006.02.048
UR - https://doi.org/10.1016/j.jpba.2006.02.048
TI - Characterization of related impurities in megestrol acetate
T2 - Journal of Pharmaceutical and Biomedical Analysis
AU - Guo, Fujiang
AU - Feng, Huijin
AU - Wang, Youfu
AU - Zhang, Chune
AU - Li, Yuanchao
PY - 2006
DA - 2006/06/01
PB - Elsevier
SP - 1418-1422
IS - 4
VL - 41
PMID - 16616448
SN - 0731-7085
SN - 1873-264X
ER -
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@article{2006_Guo,
author = {Fujiang Guo and Huijin Feng and Youfu Wang and Chune Zhang and Yuanchao Li},
title = {Characterization of related impurities in megestrol acetate},
journal = {Journal of Pharmaceutical and Biomedical Analysis},
year = {2006},
volume = {41},
publisher = {Elsevier},
month = {jun},
url = {https://doi.org/10.1016/j.jpba.2006.02.048},
number = {4},
pages = {1418--1422},
doi = {10.1016/j.jpba.2006.02.048}
}
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Guo, Fujiang, et al. “Characterization of related impurities in megestrol acetate.” Journal of Pharmaceutical and Biomedical Analysis, vol. 41, no. 4, Jun. 2006, pp. 1418-1422. https://doi.org/10.1016/j.jpba.2006.02.048.