Elsevier
Journal of Solid State Chemistry
,  volume 326 ,  pages 124222

Synthesis of cobalt molybdenum nitrides by a gas-solid reaction – In situ XRPD study

Publication type: Journal Article
Publication date: 2023-10-01
Elsevier
scimago Q2
wos Q1
SJR: 0.629
CiteScore: 6.8
Impact factor: 3.5
ISSN: 00224596, 1095726X
Materials Chemistry
Ceramics and Composites
Electronic, Optical and Magnetic Materials
Inorganic Chemistry
Physical and Theoretical Chemistry
Condensed Matter Physics
Abstract
The solid-gas reaction of the physical mixtures of cobalt(II) nitrate hexahydrate and ammonium molybdate tetrahydrate with gaseous ammonia was studied. The process was examined with the use of in situ X-ray powder diffraction (XRPD). Mixtures of cobalt molybdenum nitrides Co2Mo3N and Co3Mo3N were obtained at 700 °C. CoMoO4, Co2Mo3O8, Mo2N and metallic cobalt were identified as intermediates. The presented synthesis method allows the direct route of cobalt molybdenum nitrides formation without the wet preparation of oxidic precursor.
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Adamski P. et al. Synthesis of cobalt molybdenum nitrides by a gas-solid reaction – In situ XRPD study // Journal of Solid State Chemistry. 2023. Vol. 326. p. 124222.
GOST all authors (up to 50) Copy
Adamski P., Albrecht A., Czerwonko W., Moszyński D. Synthesis of cobalt molybdenum nitrides by a gas-solid reaction – In situ XRPD study // Journal of Solid State Chemistry. 2023. Vol. 326. p. 124222.
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RIS Copy
TY - JOUR
DO - 10.1016/j.jssc.2023.124222
UR - https://doi.org/10.1016/j.jssc.2023.124222
TI - Synthesis of cobalt molybdenum nitrides by a gas-solid reaction – In situ XRPD study
T2 - Journal of Solid State Chemistry
AU - Adamski, Paweł
AU - Albrecht, Aleksander
AU - Czerwonko, Wojciech
AU - Moszyński, Dariusz
PY - 2023
DA - 2023/10/01
PB - Elsevier
SP - 124222
VL - 326
SN - 0022-4596
SN - 1095-726X
ER -
BibTex
Cite this
BibTex (up to 50 authors) Copy
@article{2023_Adamski,
author = {Paweł Adamski and Aleksander Albrecht and Wojciech Czerwonko and Dariusz Moszyński},
title = {Synthesis of cobalt molybdenum nitrides by a gas-solid reaction – In situ XRPD study},
journal = {Journal of Solid State Chemistry},
year = {2023},
volume = {326},
publisher = {Elsevier},
month = {oct},
url = {https://doi.org/10.1016/j.jssc.2023.124222},
pages = {124222},
doi = {10.1016/j.jssc.2023.124222}
}