Spark plasma sintering of Nb/Ti3Al(Si)C2-TiC laminated composites
Egor Kashkarov
1
,
Dmitriy Krotkevich
1
,
A V Abdulmenova
1
,
A S Ivashutenko
1
,
S N Perevislov
2
,
Andrey M Lider
1
,
Nahum Travitzky
1, 3
Publication type: Journal Article
Publication date: 2023-03-01
General Materials Science
Abstract
This work describes novel Nb/Ti3Al(Si)C2-TiC laminated composites fabricated by spark plasma sintering (SPS) at 1250 °C, 50 MPa for 5 min. Preceramic papers filled with Ti3Al(Si)C2 MAX-phase and Nb foils were used as feedstock. Microstructure, phase composition and mechanical properties were evaluated by scanning electron microscopy, X-ray diffraction and three-point bending test, respectively. It was found that the reaction of preceramic paper-derived layers with Nb layers results in the formation of 16.5 µm-thick interlayers mainly composed of columnar Nb-Al intermetallic, Ti-Nb-Si and Nb-Si based phases. The laminated composites showed a brittle-ductile fracture behavior characterized by multiple deflection and branching of cracks at interfaces and plastic deformation of Nb layers. Crack deflection and delamination occur mainly near the interface between the reaction layer and ceramic layer due to the presence of more brittle silicide and carbide phases. The flexural strength of the fabricated composites was ∼350 MPa at 1.5% strain.
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Total citations:
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Citations from 2024:
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Kashkarov E. et al. Spark plasma sintering of Nb/Ti3Al(Si)C2-TiC laminated composites // Materialia. 2023. Vol. 27. p. 101673.
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Kashkarov E., Krotkevich D., Abdulmenova A. V., Ivashutenko A. S., Perevislov S. N., Lider A. M., Travitzky N. Spark plasma sintering of Nb/Ti3Al(Si)C2-TiC laminated composites // Materialia. 2023. Vol. 27. p. 101673.
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RIS
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TY - JOUR
DO - 10.1016/j.mtla.2023.101673
UR - https://doi.org/10.1016/j.mtla.2023.101673
TI - Spark plasma sintering of Nb/Ti3Al(Si)C2-TiC laminated composites
T2 - Materialia
AU - Kashkarov, Egor
AU - Krotkevich, Dmitriy
AU - Abdulmenova, A V
AU - Ivashutenko, A S
AU - Perevislov, S N
AU - Lider, Andrey M
AU - Travitzky, Nahum
PY - 2023
DA - 2023/03/01
PB - Elsevier
SP - 101673
VL - 27
SN - 2589-1529
ER -
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@article{2023_Kashkarov,
author = {Egor Kashkarov and Dmitriy Krotkevich and A V Abdulmenova and A S Ivashutenko and S N Perevislov and Andrey M Lider and Nahum Travitzky},
title = {Spark plasma sintering of Nb/Ti3Al(Si)C2-TiC laminated composites},
journal = {Materialia},
year = {2023},
volume = {27},
publisher = {Elsevier},
month = {mar},
url = {https://doi.org/10.1016/j.mtla.2023.101673},
pages = {101673},
doi = {10.1016/j.mtla.2023.101673}
}