Large acceleration of solvent-free Suzuki-Miyaura cross-coupling reactions at room temperature by the addition of small amounts of dioxane and water
Publication type: Journal Article
Publication date: 2023-06-01
scimago Q3
wos Q2
SJR: 0.426
CiteScore: 4.1
Impact factor: 2.2
ISSN: 00404020, 14645416
Organic Chemistry
Drug Discovery
Biochemistry
Abstract
The addition of small amounts of dioxane and water was quite useful in solvent-free Suzuki-Miyaura cross-coupling reactions. Various solid and liquid aryl bromides and chlorides reacted with boronic acids in the presence of 1 mol% of Pd(OAc)2 and 2 mol% of RuPhos at 25 °C to give the corresponding biaryls in good to excellent yields. The reactions of aryl chlorides proceeded faster than those of the corresponding bromides. 0.2 mol% of Pd(OAc)2 was sufficient for the reactions of some aryl chlorides. This procedure is especially useful for the reactions of aryl chlorides.
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Total citations:
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Takahashi K. Large acceleration of solvent-free Suzuki-Miyaura cross-coupling reactions at room temperature by the addition of small amounts of dioxane and water // Tetrahedron. 2023. Vol. 140. p. 133470.
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Takahashi K. Large acceleration of solvent-free Suzuki-Miyaura cross-coupling reactions at room temperature by the addition of small amounts of dioxane and water // Tetrahedron. 2023. Vol. 140. p. 133470.
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TY - JOUR
DO - 10.1016/j.tet.2023.133470
UR - https://doi.org/10.1016/j.tet.2023.133470
TI - Large acceleration of solvent-free Suzuki-Miyaura cross-coupling reactions at room temperature by the addition of small amounts of dioxane and water
T2 - Tetrahedron
AU - Takahashi, Kiyoshi
PY - 2023
DA - 2023/06/01
PB - Elsevier
SP - 133470
VL - 140
SN - 0040-4020
SN - 1464-5416
ER -
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BibTex (up to 50 authors)
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@article{2023_Takahashi,
author = {Kiyoshi Takahashi},
title = {Large acceleration of solvent-free Suzuki-Miyaura cross-coupling reactions at room temperature by the addition of small amounts of dioxane and water},
journal = {Tetrahedron},
year = {2023},
volume = {140},
publisher = {Elsevier},
month = {jun},
url = {https://doi.org/10.1016/j.tet.2023.133470},
pages = {133470},
doi = {10.1016/j.tet.2023.133470}
}