A direct transformation of O-silyl groups into O-trichloroacetates. A novel synthetic approach to protein kinase C ligands: 1-oleoyl-2-acetyl- and 1-hexadecyl-2-acetyl-sn-glycerols
2
Publication type: Journal Article
Publication date: 2005-10-01
scimago Q3
wos Q3
SJR: 0.334
CiteScore: 3.2
Impact factor: 1.5
ISSN: 00404039, 18733581
Organic Chemistry
Drug Discovery
Biochemistry
Abstract
A fluoride ion-promoted direct esterification of tert-butyldimethylsilyl- (TBDMS), or triisopropylsilyl (TIPS)-protected glycerol derivatives by means of trichloroacetic anhydride (TCAA), followed by removal of the trichloroacetyl transient protection, provides a new, efficient entry to stereochemically pure 1-oleoyl-2-acetyl- and 1-O-hexadecyl-2-acetyl-sn-glycerols.
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Stamatov S. D. et al. A direct transformation of O-silyl groups into O-trichloroacetates. A novel synthetic approach to protein kinase C ligands: 1-oleoyl-2-acetyl- and 1-hexadecyl-2-acetyl-sn-glycerols // Tetrahedron Letters. 2005. Vol. 46. No. 40. pp. 6855-6859.
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Stamatov S. D., Kullberg M., STAWIŃSKI J. A direct transformation of O-silyl groups into O-trichloroacetates. A novel synthetic approach to protein kinase C ligands: 1-oleoyl-2-acetyl- and 1-hexadecyl-2-acetyl-sn-glycerols // Tetrahedron Letters. 2005. Vol. 46. No. 40. pp. 6855-6859.
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TY - JOUR
DO - 10.1016/j.tetlet.2005.08.015
UR - https://doi.org/10.1016/j.tetlet.2005.08.015
TI - A direct transformation of O-silyl groups into O-trichloroacetates. A novel synthetic approach to protein kinase C ligands: 1-oleoyl-2-acetyl- and 1-hexadecyl-2-acetyl-sn-glycerols
T2 - Tetrahedron Letters
AU - Stamatov, Stephan D.
AU - Kullberg, Martin
AU - STAWIŃSKI, J.
PY - 2005
DA - 2005/10/01
PB - Elsevier
SP - 6855-6859
IS - 40
VL - 46
SN - 0040-4039
SN - 1873-3581
ER -
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BibTex (up to 50 authors)
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@article{2005_Stamatov,
author = {Stephan D. Stamatov and Martin Kullberg and J. STAWIŃSKI},
title = {A direct transformation of O-silyl groups into O-trichloroacetates. A novel synthetic approach to protein kinase C ligands: 1-oleoyl-2-acetyl- and 1-hexadecyl-2-acetyl-sn-glycerols},
journal = {Tetrahedron Letters},
year = {2005},
volume = {46},
publisher = {Elsevier},
month = {oct},
url = {https://doi.org/10.1016/j.tetlet.2005.08.015},
number = {40},
pages = {6855--6859},
doi = {10.1016/j.tetlet.2005.08.015}
}
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Stamatov, Stephan D., et al. “A direct transformation of O-silyl groups into O-trichloroacetates. A novel synthetic approach to protein kinase C ligands: 1-oleoyl-2-acetyl- and 1-hexadecyl-2-acetyl-sn-glycerols.” Tetrahedron Letters, vol. 46, no. 40, Oct. 2005, pp. 6855-6859. https://doi.org/10.1016/j.tetlet.2005.08.015.