An improved procedure for the separation of (+) or (−)-isopinocampheol, the major side product of the oxidation workup procedure of Brown’s asymmetric crotylborations
Publication type: Journal Article
Publication date: 2007-10-01
scimago Q3
wos Q3
SJR: 0.334
CiteScore: 3.2
Impact factor: 1.5
ISSN: 00404039, 18733581
Organic Chemistry
Drug Discovery
Biochemistry
Abstract
Separation of (+) or (−)-isopinocampheol, the major side product of the oxidation workup procedure of Brown’s asymmetric reactions such as crotylborations from the desired product is quite tedious and often requires repeated column chromatography. It is discovered that a sublimation process can be used to easily separate this major side product.
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Hua Z., Jin Z. An improved procedure for the separation of (+) or (−)-isopinocampheol, the major side product of the oxidation workup procedure of Brown’s asymmetric crotylborations // Tetrahedron Letters. 2007. Vol. 48. No. 43. pp. 7695-7697.
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Hua Z., Jin Z. An improved procedure for the separation of (+) or (−)-isopinocampheol, the major side product of the oxidation workup procedure of Brown’s asymmetric crotylborations // Tetrahedron Letters. 2007. Vol. 48. No. 43. pp. 7695-7697.
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TY - JOUR
DO - 10.1016/j.tetlet.2007.08.075
UR - https://doi.org/10.1016/j.tetlet.2007.08.075
TI - An improved procedure for the separation of (+) or (−)-isopinocampheol, the major side product of the oxidation workup procedure of Brown’s asymmetric crotylborations
T2 - Tetrahedron Letters
AU - Hua, Zhengmao
AU - Jin, Zhen-Dong
PY - 2007
DA - 2007/10/01
PB - Elsevier
SP - 7695-7697
IS - 43
VL - 48
SN - 0040-4039
SN - 1873-3581
ER -
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BibTex (up to 50 authors)
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@article{2007_Hua,
author = {Zhengmao Hua and Zhen-Dong Jin},
title = {An improved procedure for the separation of (+) or (−)-isopinocampheol, the major side product of the oxidation workup procedure of Brown’s asymmetric crotylborations},
journal = {Tetrahedron Letters},
year = {2007},
volume = {48},
publisher = {Elsevier},
month = {oct},
url = {https://doi.org/10.1016/j.tetlet.2007.08.075},
number = {43},
pages = {7695--7697},
doi = {10.1016/j.tetlet.2007.08.075}
}
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MLA
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Hua, Zhengmao, and Zhen-Dong Jin. “An improved procedure for the separation of (+) or (−)-isopinocampheol, the major side product of the oxidation workup procedure of Brown’s asymmetric crotylborations.” Tetrahedron Letters, vol. 48, no. 43, Oct. 2007, pp. 7695-7697. https://doi.org/10.1016/j.tetlet.2007.08.075.