Mono-acylation of piperazine and homopiperazine via ionic immobilization
1
Neurogen Corporation, 35 Northeast Industrial Road, Branford, CT 06405, United States
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Publication type: Journal Article
Publication date: 2008-08-01
scimago Q3
wos Q3
SJR: 0.334
CiteScore: 3.2
Impact factor: 1.5
ISSN: 00404039, 18733581
Organic Chemistry
Drug Discovery
Biochemistry
Abstract
A method for the selective mono-acylation of piperazine and homopiperazine has been developed. In a flow system, initially the diamine is ionically immobilized on a sulfonic acid funtionalized silica gel, acylated with an appropriate reagent and finally liberated with ammonic methanol. Examples with high yield and purity are presented.
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11
Total citations:
11
Citations from 2024:
1
(9.09%)
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MLA
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GOST
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Pringle W. Mono-acylation of piperazine and homopiperazine via ionic immobilization // Tetrahedron Letters. 2008. Vol. 49. No. 34. pp. 5047-5049.
GOST all authors (up to 50)
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Pringle W. Mono-acylation of piperazine and homopiperazine via ionic immobilization // Tetrahedron Letters. 2008. Vol. 49. No. 34. pp. 5047-5049.
Cite this
RIS
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TY - JOUR
DO - 10.1016/j.tetlet.2008.06.044
UR - https://doi.org/10.1016/j.tetlet.2008.06.044
TI - Mono-acylation of piperazine and homopiperazine via ionic immobilization
T2 - Tetrahedron Letters
AU - Pringle, Wallace
PY - 2008
DA - 2008/08/01
PB - Elsevier
SP - 5047-5049
IS - 34
VL - 49
SN - 0040-4039
SN - 1873-3581
ER -
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BibTex (up to 50 authors)
Copy
@article{2008_Pringle,
author = {Wallace Pringle},
title = {Mono-acylation of piperazine and homopiperazine via ionic immobilization},
journal = {Tetrahedron Letters},
year = {2008},
volume = {49},
publisher = {Elsevier},
month = {aug},
url = {https://doi.org/10.1016/j.tetlet.2008.06.044},
number = {34},
pages = {5047--5049},
doi = {10.1016/j.tetlet.2008.06.044}
}
Cite this
MLA
Copy
Pringle, Wallace. “Mono-acylation of piperazine and homopiperazine via ionic immobilization.” Tetrahedron Letters, vol. 49, no. 34, Aug. 2008, pp. 5047-5049. https://doi.org/10.1016/j.tetlet.2008.06.044.