Synthesis of 2-amino-2-deoxy-d-mannuronic acid and some derivatives thereof
Тип публикации: Journal Article
Дата публикации: 1970-02-01
SCImago Q2
WOS Q1
БС2
SJR: 0.483
CiteScore: 3.7
Impact factor: 3.4
ISSN: 00086215, 1873426X
Organic Chemistry
Biochemistry
General Medicine
Analytical Chemistry
Краткое описание
2-Amino-2-deoxy- d -mannose hydrochloride was converted into the N -benzyl-oxycarbonyl derivative ( 2 ) by treatment with benzyl chloroformate in ethanol-water at pH 7.0. Benzyl 2-(benzyloxycarbonyl)amino-2-deoxy-α- d -mannoside, obtained from 2 by treatment with benzyl alcohol containing 2% of hydrogen chloride, was oxidized with oxygen in the presence of a platinum catalyst to benzyl 2-(benzyl-oxycarbonyl)amino-2-deoxy-α- d -mannopyranosiduronic acid ( 4 ). Periodate oxidation showed that 4 had a pyranoid structure. Hydrogenolysis of the uronic acid 4 in the presence of a palladium-carbon catalyst gave 2-amino-2-deoxy- d -mannuronic acid ( 5 ), which differed from its 2-epimer (2-amino-2-deoxy- d -glucuronic acid) in its optical rotation, and paper chromatographic and electrophoretic behavior.
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ГОСТ
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Kundu N. G. et al. Synthesis of 2-amino-2-deoxy-d-mannuronic acid and some derivatives thereof // Carbohydrate Research. 1970. Vol. 12. No. 2. pp. 225-232.
ГОСТ со всеми авторами (до 50)
Скопировать
Kundu N. G., Crawfor J. F., Prajsnar B., Reed E. J., Rosenthal S. Synthesis of 2-amino-2-deoxy-d-mannuronic acid and some derivatives thereof // Carbohydrate Research. 1970. Vol. 12. No. 2. pp. 225-232.
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RIS
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TY - JOUR
DO - 10.1016/s0008-6215(00)80100-7
UR - https://doi.org/10.1016/s0008-6215(00)80100-7
TI - Synthesis of 2-amino-2-deoxy-d-mannuronic acid and some derivatives thereof
T2 - Carbohydrate Research
AU - Kundu, Nitya G.
AU - Crawfor, John F
AU - Prajsnar, Bronislaw
AU - Reed, Elizabeth J
AU - Rosenthal, Spencer
PY - 1970
DA - 1970/02/01
PB - Elsevier
SP - 225-232
IS - 2
VL - 12
SN - 0008-6215
SN - 1873-426X
ER -
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BibTex (до 50 авторов)
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@article{1970_Kundu,
author = {Nitya G. Kundu and John F Crawfor and Bronislaw Prajsnar and Elizabeth J Reed and Spencer Rosenthal},
title = {Synthesis of 2-amino-2-deoxy-d-mannuronic acid and some derivatives thereof},
journal = {Carbohydrate Research},
year = {1970},
volume = {12},
publisher = {Elsevier},
month = {feb},
url = {https://doi.org/10.1016/s0008-6215(00)80100-7},
number = {2},
pages = {225--232},
doi = {10.1016/s0008-6215(00)80100-7}
}
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MLA
Скопировать
Kundu, Nitya G., et al. “Synthesis of 2-amino-2-deoxy-d-mannuronic acid and some derivatives thereof.” Carbohydrate Research, vol. 12, no. 2, Feb. 1970, pp. 225-232. https://doi.org/10.1016/s0008-6215(00)80100-7.
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