Crystal and molecular structure of tetrakis(N-ethylthiourea)platinum(II) iodide
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Laboratorio di Strutturistica Chimica “Giordano Giacomello”, C.N.R., Area della Ricerca, C.P. 10, 00016 Monterotondo Stazione, Roma, Italy
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Тип публикации: Journal Article
Дата публикации: 1976-01-01
scimago Q3
wos Q2
БС2
SJR: 0.393
CiteScore: 5.5
Impact factor: 3.2
ISSN: 00201693, 18733255
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Краткое описание
The crystal structure of tetrakis(N-ethylthiourea)platinum(II) iodide, [Pt(CS(NH2)(NHC2H5))4]I2, has been determined from three-dimensional X-ray diffraction data. The triclinic crystals belong to the P 1 space group: a = 8.096(8), b = 13.165(12), c = 14.248 (12) A, α = 101.7(1), β = 108.5(1), γ = 102.1(1)°. The observed and calculated (Z = 2) densities are 2.13(1) and 2.127 g cm−3 respectively. 5306 independent reflections with Fo2 > 3σ(Fo2) were collected by counter methods. Least-squares refinement gave a final discrepancy factor of 0.038. The stereochemistry around the platinum is almost square-planar with the sulphur atom of each thiourea group bound to the metal. Pt-S distances range from 2.309(3) to 2.335 (3) A. The thiourea groups have quite regular geometry and dimensions. The structure is stabilized in the solid state by a network of NH … I−1 hydrogen bonds.
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Bachechi F., Zambonelli L., Marcotrigiano G. Crystal and molecular structure of tetrakis(N-ethylthiourea)platinum(II) iodide // Inorganica Chimica Acta. 1976. Vol. 17. pp. 225-228.
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Bachechi F., Zambonelli L., Marcotrigiano G. Crystal and molecular structure of tetrakis(N-ethylthiourea)platinum(II) iodide // Inorganica Chimica Acta. 1976. Vol. 17. pp. 225-228.
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TY - JOUR
DO - 10.1016/s0020-1693(00)81986-6
UR - https://doi.org/10.1016/s0020-1693(00)81986-6
TI - Crystal and molecular structure of tetrakis(N-ethylthiourea)platinum(II) iodide
T2 - Inorganica Chimica Acta
AU - Bachechi, F.
AU - Zambonelli, L.
AU - Marcotrigiano, G.
PY - 1976
DA - 1976/01/01
PB - Elsevier
SP - 225-228
VL - 17
SN - 0020-1693
SN - 1873-3255
ER -
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@article{1976_Bachechi,
author = {F. Bachechi and L. Zambonelli and G. Marcotrigiano},
title = {Crystal and molecular structure of tetrakis(N-ethylthiourea)platinum(II) iodide},
journal = {Inorganica Chimica Acta},
year = {1976},
volume = {17},
publisher = {Elsevier},
month = {jan},
url = {https://doi.org/10.1016/s0020-1693(00)81986-6},
pages = {225--228},
doi = {10.1016/s0020-1693(00)81986-6}
}