Selenocyanation using a combined reagent of triphenylphosphine and selenocyanogen. A new and simple synthesis of alkyl selenocyanates and symmetrical alkyl diselenides from alcohols
Тип публикации: Journal Article
Дата публикации: 1979-01-01
SCImago Q3
WOS Q3
БС2
SJR: 0.285
CiteScore: 2.8
Impact factor: 1.4
ISSN: 00404039, 18733581
Organic Chemistry
Drug Discovery
Biochemistry
Краткое описание
A novel reagent Ph 3 SeCN) 2 , easily prepared by adding an equimolar amount of tri-phenylphosphine to selenocyanogen solution in methylene chloride and tetrahydrofuran reacts below −60° with primary alcohols to produce directly the corresponding alkyl selenocyanates and alkyl diselenides in good yields. With secondary alcohols mixtures of selenocyanates and isoselenocyanates are obtained, while tertiary alcohols fail to react with the reagent.
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ГОСТ
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Tamura Y. et al. Selenocyanation using a combined reagent of triphenylphosphine and selenocyanogen. A new and simple synthesis of alkyl selenocyanates and symmetrical alkyl diselenides from alcohols // Tetrahedron Letters. 1979. Vol. 20. No. 24. pp. 2251-2252.
ГОСТ со всеми авторами (до 50)
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Tamura Y., Adachi M., Kawasaki T., Kita Y. Selenocyanation using a combined reagent of triphenylphosphine and selenocyanogen. A new and simple synthesis of alkyl selenocyanates and symmetrical alkyl diselenides from alcohols // Tetrahedron Letters. 1979. Vol. 20. No. 24. pp. 2251-2252.
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RIS
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TY - JOUR
DO - 10.1016/s0040-4039(01)93689-5
UR - https://doi.org/10.1016/s0040-4039(01)93689-5
TI - Selenocyanation using a combined reagent of triphenylphosphine and selenocyanogen. A new and simple synthesis of alkyl selenocyanates and symmetrical alkyl diselenides from alcohols
T2 - Tetrahedron Letters
AU - Tamura, Y.
AU - Adachi, M.
AU - Kawasaki, T.
AU - Kita, Y.
PY - 1979
DA - 1979/01/01
PB - Elsevier
SP - 2251-2252
IS - 24
VL - 20
SN - 0040-4039
SN - 1873-3581
ER -
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BibTex (до 50 авторов)
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@article{1979_Tamura,
author = {Y. Tamura and M. Adachi and T. Kawasaki and Y. Kita},
title = {Selenocyanation using a combined reagent of triphenylphosphine and selenocyanogen. A new and simple synthesis of alkyl selenocyanates and symmetrical alkyl diselenides from alcohols},
journal = {Tetrahedron Letters},
year = {1979},
volume = {20},
publisher = {Elsevier},
month = {jan},
url = {https://doi.org/10.1016/s0040-4039(01)93689-5},
number = {24},
pages = {2251--2252},
doi = {10.1016/s0040-4039(01)93689-5}
}
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MLA
Скопировать
Tamura, Y., et al. “Selenocyanation using a combined reagent of triphenylphosphine and selenocyanogen. A new and simple synthesis of alkyl selenocyanates and symmetrical alkyl diselenides from alcohols.” Tetrahedron Letters, vol. 20, no. 24, Jan. 1979, pp. 2251-2252. https://doi.org/10.1016/s0040-4039(01)93689-5.
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