Journal of Non-Crystalline Solids, volume 126, issue 1-2, pages 87-92
Microcrystalline PbS doped silica glasses prepared by the sol-gel process
2
Industrial Research Institute, Aichi Prefectural Government, Hitotsugi, Kariya 448, Japan
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Publication type: Journal Article
Publication date: 1990-12-01
Journal:
Journal of Non-Crystalline Solids
Q2
Q2
SJR: 0.655
CiteScore: 6.5
Impact factor: 3.2
ISSN: 00223093, 18734812
Materials Chemistry
Ceramics and Composites
Electronic, Optical and Magnetic Materials
Condensed Matter Physics
Abstract
The sol-gel process has been applied to the preparation of small size PbS crystal doped silica glasses. Silica glasses containing 1.8 and 4.5 wt% PbO were prepared by hydrolysis of Si(OC 2 H 5 ) 4 and Pb(CH 3 COO) 2 ·3H 2 O and subsequent reaction with H 2 S gas to form fine, cubic PbS microcrystal doped glasses. The microcrystal size (2 to 10 nm in diameter) was dependent on H 2 S gas reaction temperature. The absorption edge exhibited a blue shift of ∼ 2.0 eV from that of the bulk PbS crystal. Thus the quantum size effect was found for glasses containing PbS prepared by the sol-gel process.
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GOST
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Nogami M. et al. Microcrystalline PbS doped silica glasses prepared by the sol-gel process // Journal of Non-Crystalline Solids. 1990. Vol. 126. No. 1-2. pp. 87-92.
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Nogami M., NAGASAKA K., Kotani K. Microcrystalline PbS doped silica glasses prepared by the sol-gel process // Journal of Non-Crystalline Solids. 1990. Vol. 126. No. 1-2. pp. 87-92.
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RIS
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TY - JOUR
DO - 10.1016/0022-3093(90)91026-N
UR - https://doi.org/10.1016/0022-3093(90)91026-N
TI - Microcrystalline PbS doped silica glasses prepared by the sol-gel process
T2 - Journal of Non-Crystalline Solids
AU - Nogami, Masayuki
AU - NAGASAKA, Katsumi
AU - Kotani, Keiko
PY - 1990
DA - 1990/12/01
PB - Elsevier
SP - 87-92
IS - 1-2
VL - 126
SN - 0022-3093
SN - 1873-4812
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{1990_Nogami,
author = {Masayuki Nogami and Katsumi NAGASAKA and Keiko Kotani},
title = {Microcrystalline PbS doped silica glasses prepared by the sol-gel process},
journal = {Journal of Non-Crystalline Solids},
year = {1990},
volume = {126},
publisher = {Elsevier},
month = {dec},
url = {https://doi.org/10.1016/0022-3093(90)91026-N},
number = {1-2},
pages = {87--92},
doi = {10.1016/0022-3093(90)91026-N}
}
Cite this
MLA
Copy
Nogami, Masayuki, et al. “Microcrystalline PbS doped silica glasses prepared by the sol-gel process.” Journal of Non-Crystalline Solids, vol. 126, no. 1-2, Dec. 1990, pp. 87-92. https://doi.org/10.1016/0022-3093(90)91026-N.