Synthesis of 1-cyclopropylmethylsilatrane and 1-cyclopropylmethyl-3,7,10-trimethylsilatrane. Crystal structure of 1-cyclopropylmethylsilatrane
Тип публикации: Journal Article
Дата публикации: 1996-10-01
scimago Q3
wos Q2
БС2
SJR: 0.385
CiteScore: 4.1
Impact factor: 2.4
ISSN: 0022328X, 18728561
Materials Chemistry
Organic Chemistry
Biochemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Краткое описание
Abstract 1-Cyclopropylmethylsilatrane ( 2a ) and 1-cyclopropylmethyl-3,7,10-trimethylsilatrane ( 2b ) have been prepared in good yields by the reaction of the corresponding 1-allylsilatranes N(CH 2 CHRO) 3 SiCH 2 CHCH 2 ( 1 ) (R H ( a ), Me ( b )) with diazomethane in the presence of Pd(OAc) 2 as a catalyst. 1-Cyclopropylmethylsilatrane ( 2a ) has also been synthesized from the reaction of cyclopropylmethyltriethoxysilane ( 3 ) with triethanolamine. Compounds 2a, 2b and 3 have been characterized by 1 H and 13 C NMR spectroscopy and elemental analyses. An X-ray structure determination of 2a indicates the presence of an N → Si bond length of 2.149(4) A.
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Zaitseva G. S. et al. Synthesis of 1-cyclopropylmethylsilatrane and 1-cyclopropylmethyl-3,7,10-trimethylsilatrane. Crystal structure of 1-cyclopropylmethylsilatrane // Journal of Organometallic Chemistry. 1996. Vol. 523. No. 2. pp. 221-225.
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Zaitseva G. S., Karlov S. S., Churakov A. V., Avtomonov E. V., Lorberth J., Hertel D. Synthesis of 1-cyclopropylmethylsilatrane and 1-cyclopropylmethyl-3,7,10-trimethylsilatrane. Crystal structure of 1-cyclopropylmethylsilatrane // Journal of Organometallic Chemistry. 1996. Vol. 523. No. 2. pp. 221-225.
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TY - JOUR
DO - 10.1016/0022-328X(96)06430-3
UR - https://linkinghub.elsevier.com/retrieve/pii/0022328X96064303
TI - Synthesis of 1-cyclopropylmethylsilatrane and 1-cyclopropylmethyl-3,7,10-trimethylsilatrane. Crystal structure of 1-cyclopropylmethylsilatrane
T2 - Journal of Organometallic Chemistry
AU - Zaitseva, Galina S.
AU - Karlov, Sergey S.
AU - Churakov, Andrei V.
AU - Avtomonov, Evgeni V
AU - Lorberth, Jörg
AU - Hertel, Dirk
PY - 1996
DA - 1996/10/01
PB - Elsevier
SP - 221-225
IS - 2
VL - 523
SN - 0022-328X
SN - 1872-8561
ER -
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@article{1996_Zaitseva,
author = {Galina S. Zaitseva and Sergey S. Karlov and Andrei V. Churakov and Evgeni V Avtomonov and Jörg Lorberth and Dirk Hertel},
title = {Synthesis of 1-cyclopropylmethylsilatrane and 1-cyclopropylmethyl-3,7,10-trimethylsilatrane. Crystal structure of 1-cyclopropylmethylsilatrane},
journal = {Journal of Organometallic Chemistry},
year = {1996},
volume = {523},
publisher = {Elsevier},
month = {oct},
url = {https://linkinghub.elsevier.com/retrieve/pii/0022328X96064303},
number = {2},
pages = {221--225},
doi = {10.1016/0022-328X(96)06430-3}
}
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MLA
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Zaitseva, Galina S., et al. “Synthesis of 1-cyclopropylmethylsilatrane and 1-cyclopropylmethyl-3,7,10-trimethylsilatrane. Crystal structure of 1-cyclopropylmethylsilatrane.” Journal of Organometallic Chemistry, vol. 523, no. 2, Oct. 1996, pp. 221-225. https://linkinghub.elsevier.com/retrieve/pii/0022328X96064303.
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