Journal of Solid State Chemistry, volume 43, issue 2, pages 151-162
Synthese, structure cristalline et analyse vibrationnelle de l'hexathiohypodiphosphate de lithium Li4P2S6
1
Laboratoire d'Electrochimie des Solides - ERA 810 Université de Franche-Comté 25030 Besancon Cedex France
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2
Laboratoire de Chimie Physique, Université de Franche-Comté, 25030 Besancon Cedex, France
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Publication type: Journal Article
Publication date: 1982-07-01
Journal:
Journal of Solid State Chemistry
Quartile SCImago
Q2
Quartile WOS
Q2
Impact factor: 3.3
ISSN: 00224596, 1095726X
Materials Chemistry
Ceramics and Composites
Electronic, Optical and Magnetic Materials
Inorganic Chemistry
Physical and Theoretical Chemistry
Condensed Matter Physics
Abstract
Resume Le compose Li4P2S6 est obtenu soit par devitrification du verre Li4P2S7 a 450°C avec formation de soufre soit par fusion d'un melange Li2S, P et S et cristallisation a 450°C. La structure a ete determinee par diffraction X sur monocristal. La maille elementaire est hexagonale P6 3 mcm avec a = 6,070(4), c = 6,577(4) A, V = 209 A3, Z = 1. La mesure a 293°K des intensites a ete realisee sur un diffractometre Nonius CAD-4 avec la radiation Kα d'un tube a anticathode de molybdene (λ = 0,71069 A). La structure a ete resolue en admettant un desordre statistique des atomes P sur deux sites (taux d'occupation de 1 2 ). L'affinement de neuf parametres sur 90 reflexions independantes conduit a un facteur d'accord R de 0,047. La structure resulte d'un empilement d'atomes de soufre suivant une sequence ABAB. Quatre des six sites octaedriques de chaque maille sont occupes par des ions Li+; les deux autres sont remplis statistiquement (0,5) par des paires PP. L'anion P2S4−6 de symetrie D3d est forme par deux groupes PS3 (PS = 2,032(5) A) en configuration decalee avec une liaison centrale PP(2,256(13) A). Les spectres ir et Raman presentent des similitudes avec ceux de Na4P2S6, 6H2O et des composes MIIPS3. Une nouvelle attribution en terme de types de symetrie est proposee pour les modes internes de P2S6; un calcul des coordonnees normales utilisant un champ de forces de valence confirme cette attribution; les constantes de force fPP et fPS sont respectivement egales a 1,6 et 2,7 mdyne A−1.
Top-30
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Citations by publishers
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5
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35
40
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Elsevier
36 publications, 34.62%
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American Chemical Society (ACS)
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Royal Society of Chemistry (RSC)
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American Physical Society (APS)
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Walter de Gruyter
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World Scientific
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Physical Society of Japan
1 publication, 0.96%
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Frontiers Media S.A.
1 publication, 0.96%
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Cambridge University Press
1 publication, 0.96%
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IOP Publishing
1 publication, 0.96%
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Chemical Industry Press
1 publication, 0.96%
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1 publication, 0.96%
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1 publication, 0.96%
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1 publication, 0.96%
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5
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- We do not take into account publications without a DOI.
- Statistics recalculated only for publications connected to researchers, organizations and labs registered on the platform.
- Statistics recalculated weekly.
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Mercier R. et al. Synthese, structure cristalline et analyse vibrationnelle de l'hexathiohypodiphosphate de lithium Li4P2S6 // Journal of Solid State Chemistry. 1982. Vol. 43. No. 2. pp. 151-162.
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Mercier R., Malugani J., Fahys B., Douglande J., Robert G. Synthese, structure cristalline et analyse vibrationnelle de l'hexathiohypodiphosphate de lithium Li4P2S6 // Journal of Solid State Chemistry. 1982. Vol. 43. No. 2. pp. 151-162.
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TY - JOUR
DO - 10.1016/0022-4596(82)90224-9
UR - https://doi.org/10.1016/0022-4596(82)90224-9
TI - Synthese, structure cristalline et analyse vibrationnelle de l'hexathiohypodiphosphate de lithium Li4P2S6
T2 - Journal of Solid State Chemistry
AU - Mercier, R.
AU - Malugani, J.-P.
AU - Fahys, B.
AU - Douglande, J
AU - Robert, G.
PY - 1982
DA - 1982/07/01 00:00:00
PB - Elsevier
SP - 151-162
IS - 2
VL - 43
SN - 0022-4596
SN - 1095-726X
ER -
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@article{1982_Mercier,
author = {R. Mercier and J.-P. Malugani and B. Fahys and J Douglande and G. Robert},
title = {Synthese, structure cristalline et analyse vibrationnelle de l'hexathiohypodiphosphate de lithium Li4P2S6},
journal = {Journal of Solid State Chemistry},
year = {1982},
volume = {43},
publisher = {Elsevier},
month = {jul},
url = {https://doi.org/10.1016/0022-4596(82)90224-9},
number = {2},
pages = {151--162},
doi = {10.1016/0022-4596(82)90224-9}
}
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MLA
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Mercier, R., et al. “Synthese, structure cristalline et analyse vibrationnelle de l'hexathiohypodiphosphate de lithium Li4P2S6.” Journal of Solid State Chemistry, vol. 43, no. 2, Jul. 1982, pp. 151-162. https://doi.org/10.1016/0022-4596(82)90224-9.