Journal of Solid State Chemistry, volume 83, issue 1, pages 78-90
Dimorphism, phase transitions, and transport properties in LiZr2(PO4)3
1
Groupe de Chimie du Solide, Laboratoire de Physique de la Matière Condensée, Ecole Polytechnique, 91128 Palaiseau Cedex, France
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Publication type: Journal Article
Publication date: 1989-11-01
Journal:
Journal of Solid State Chemistry
Quartile SCImago
Q2
Quartile WOS
Q2
Impact factor: 3.3
ISSN: 00224596, 1095726X
Materials Chemistry
Ceramics and Composites
Electronic, Optical and Magnetic Materials
Inorganic Chemistry
Physical and Theoretical Chemistry
Condensed Matter Physics
Abstract
The authors report the structure, the phase transitions, and the transport properties of two different phases of LiZr{sub 2}(PO{sub 4}){sub 3} materials prepared by the sol/gel technique. The phase have been characterized by X-ray powder diffractometry, thermal analysis, ac conductivity, and NMR ({sup 31}P and {sup 7}Li). A high-temperature phase, prepared at 1,200{degree}C, shows a NASICON-type structure and a monoclinic {yields} rhombohedral first order transition at about 40{degree}C. This transformation is associated with the sharp appearance of a lithium motion leading to high conducting properties above the phase transition {sigma} = 1.2.10{sup {minus}2} ({Omega} cm){sup {minus}1} at 300{degree}C. A low-temperature phase, prepared at 900{degree}C, exhibits the {beta}-Fe{sub 2}(SO{sub 4}){sub 3}-type structure and a monoclinic {yields} orthorhombic transformation at 300{degree}C. A local lithium motion progressively takes place between RT and 120{degree}C and a conducting state is observed at 300{degree}C ({sigma} =5.10{sup {minus}4} ({Omega} cm){sup {minus}1}). In diphasic samples prepared between 900 and 1200{degree}C, both resistivity and activation energy progressively increase with the low-high temperature phase ratio.
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- We do not take into account publications without a DOI.
- Statistics recalculated only for publications connected to researchers, organizations and labs registered on the platform.
- Statistics recalculated weekly.
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Sudreau F., PETIT D., Boilot J. P. Dimorphism, phase transitions, and transport properties in LiZr2(PO4)3 // Journal of Solid State Chemistry. 1989. Vol. 83. No. 1. pp. 78-90.
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Sudreau F., PETIT D., Boilot J. P. Dimorphism, phase transitions, and transport properties in LiZr2(PO4)3 // Journal of Solid State Chemistry. 1989. Vol. 83. No. 1. pp. 78-90.
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TY - JOUR
DO - 10.1016/0022-4596(89)90056-X
UR - https://doi.org/10.1016/0022-4596(89)90056-X
TI - Dimorphism, phase transitions, and transport properties in LiZr2(PO4)3
T2 - Journal of Solid State Chemistry
AU - Sudreau, F
AU - PETIT, D.
AU - Boilot, J. P.
PY - 1989
DA - 1989/11/01 00:00:00
PB - Elsevier
SP - 78-90
IS - 1
VL - 83
SN - 0022-4596
SN - 1095-726X
ER -
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@article{1989_Sudreau,
author = {F Sudreau and D. PETIT and J. P. Boilot},
title = {Dimorphism, phase transitions, and transport properties in LiZr2(PO4)3},
journal = {Journal of Solid State Chemistry},
year = {1989},
volume = {83},
publisher = {Elsevier},
month = {nov},
url = {https://doi.org/10.1016/0022-4596(89)90056-X},
number = {1},
pages = {78--90},
doi = {10.1016/0022-4596(89)90056-X}
}
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Sudreau, F., et al. “Dimorphism, phase transitions, and transport properties in LiZr2(PO4)3.” Journal of Solid State Chemistry, vol. 83, no. 1, Nov. 1989, pp. 78-90. https://doi.org/10.1016/0022-4596(89)90056-X.