Physica C: Superconductivity and its Applications

, том 215 , издание 1-2 , страницы 1-10

The synthesis and characterization of the HgBa2Ca2Cu3O8+δ and HgBa2Ca3Cu4O10+δ phases

Тип публикации: Journal Article

Дата публикации: 1993-09-01

Elsevier

Physica C: Superconductivity and its Applications

scimago Q3

wos Q4

БС3

SJR: 0.313

CiteScore: 2.4

Impact factor: 1.0

ISSN: 09214534, 18732143

DOI: 10.1016/0921-4534(93)90358-W

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Electronic, Optical and Magnetic Materials

Condensed Matter Physics

Electrical and Electronic Engineering

Energy Engineering and Power Technology

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Abstract The third (Hg-1223) and the fourth (Hg-1234) members of the recently-discovered homologous series HgBa2Can−1CunO2n+2+δ have been synthesized by solid state reaction, carried out at 950°C under 50 kbar at different annealing times. These phases have a tetragonal cell with lattice parameters: a = 3.8532 (6) A , c = 15.818(2) A , and a = 3.8540(3) A , c = 19.006 (3) A , respectively. The c parameters are in agreement with the formula c ≌ 9.5 + 3.2 (n − 1). Electron microscopy study showed similar lattice parameters as well as the occurence of different intergrowths and stacking faults. A periodicity of 22 A has also been detected, which may be attributed to the existence of the Hg-1245 phase. EDS analysis data of several grains of Hg-1223 and Hg-1234 are in agreement with the proposed chemical formulae. AC susceptibility measurements show that an increase of the superconducting transition temperature with n in the HgBa2Can−1CunO2n+2+δ series occurs till the third member, after which a saturation seems to be achieved.

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Антипов Евгений

д.х.н., проф., академик, Российская академия наук

466 публикаций, 10 708 цитирований, 29 рецензий

Индекс Хирша: 50

Московский государственный университет имени М.В. Ломоносова

Сколковский институт науки и технологий

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Antipov E. V. et al. The synthesis and characterization of the HgBa2Ca2Cu3O8+δ and HgBa2Ca3Cu4O10+δ phases // Physica C: Superconductivity and its Applications. 1993. Vol. 215. No. 1-2. pp. 1-10.

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Antipov E. V., Loureiro S. M., Chaillout C., Capponi J., Bordet P., Tholence J. L., Putilin S. N., MAREZIO M. The synthesis and characterization of the HgBa2Ca2Cu3O8+δ and HgBa2Ca3Cu4O10+δ phases // Physica C: Superconductivity and its Applications. 1993. Vol. 215. No. 1-2. pp. 1-10.

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TY - JOUR

DO - 10.1016/0921-4534(93)90358-W

UR - https://linkinghub.elsevier.com/retrieve/pii/092145349390358W

TI - The synthesis and characterization of the HgBa2Ca2Cu3O8+δ and HgBa2Ca3Cu4O10+δ phases

T2 - Physica C: Superconductivity and its Applications

AU - Antipov, Evgeny V.

AU - Loureiro, S. M.

AU - Chaillout, C.

AU - Capponi, J.J.

AU - Bordet, Pierre

AU - Tholence, J. L.

AU - Putilin, S. N.

AU - MAREZIO, M.

PY - 1993

DA - 1993/09/01

PB - Elsevier

SP - 1-10

IS - 1-2

VL - 215

SN - 0921-4534

SN - 1873-2143

ER -

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@article{1993_Antipov,

author = {Evgeny V. Antipov and S. M. Loureiro and C. Chaillout and J.J. Capponi and Pierre Bordet and J. L. Tholence and S. N. Putilin and M. MAREZIO},

title = {The synthesis and characterization of the HgBa2Ca2Cu3O8+δ and HgBa2Ca3Cu4O10+δ phases},

journal = {Physica C: Superconductivity and its Applications},

year = {1993},

volume = {215},

publisher = {Elsevier},

month = {sep},

url = {https://linkinghub.elsevier.com/retrieve/pii/092145349390358W},

number = {1-2},

pages = {1--10},

doi = {10.1016/0921-4534(93)90358-W}

}

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Antipov, Evgeny V., et al. “The synthesis and characterization of the HgBa2Ca2Cu3O8+δ and HgBa2Ca3Cu4O10+δ phases.” Physica C: Superconductivity and its Applications, vol. 215, no. 1-2, Sep. 1993, pp. 1-10. https://linkinghub.elsevier.com/retrieve/pii/092145349390358W.