Synthesis and x-ray crystal structure of a tin(IV) tetrahalide adduct with a crown ether
Тип публикации: Journal Article
Дата публикации: 1984-02-01
scimago Q3
wos Q2
БС2
SJR: 0.393
CiteScore: 5.5
Impact factor: 3.2
ISSN: 00201693, 18733255
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Краткое описание
The polymeric structure of the complex, [SnCl4(H2O)2]18-crown-6·2H2O, prepared by the addition of a solution of SnCl4 to 18-crown-6, has been determined by X-ray analysis. The structure has been solved by three-dimensional Patterson-Fourier synthesis to a conventional R-factor of 0.13, by using 1394 reflections with I>3σ(I). The crystals are monoclinic, with a = 15.753(3), b = 15.072(3), c = 12.209(4), β = 97.77°(1.0), z = 4, and space group P21/a. The tin atom is octahedrally coordinated to four chlorine atoms and two water molecules in cis positions. A very complex network of hydrogen bonding links together the tin coordination octahedron, the two water hydration molecules, and the two crystallographically-different half crown-ethers.
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Valle G., Cassol A., Russo U. Synthesis and x-ray crystal structure of a tin(IV) tetrahalide adduct with a crown ether // Inorganica Chimica Acta. 1984. Vol. 82. No. 1. pp. 81-84.
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Valle G., Cassol A., Russo U. Synthesis and x-ray crystal structure of a tin(IV) tetrahalide adduct with a crown ether // Inorganica Chimica Acta. 1984. Vol. 82. No. 1. pp. 81-84.
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TY - JOUR
DO - 10.1016/S0020-1693(00)82542-6
UR - https://doi.org/10.1016/S0020-1693(00)82542-6
TI - Synthesis and x-ray crystal structure of a tin(IV) tetrahalide adduct with a crown ether
T2 - Inorganica Chimica Acta
AU - Valle, Giovanni
AU - Cassol, Alberto
AU - Russo, Umberto
PY - 1984
DA - 1984/02/01
PB - Elsevier
SP - 81-84
IS - 1
VL - 82
SN - 0020-1693
SN - 1873-3255
ER -
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BibTex (до 50 авторов)
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@article{1984_Valle,
author = {Giovanni Valle and Alberto Cassol and Umberto Russo},
title = {Synthesis and x-ray crystal structure of a tin(IV) tetrahalide adduct with a crown ether},
journal = {Inorganica Chimica Acta},
year = {1984},
volume = {82},
publisher = {Elsevier},
month = {feb},
url = {https://doi.org/10.1016/S0020-1693(00)82542-6},
number = {1},
pages = {81--84},
doi = {10.1016/S0020-1693(00)82542-6}
}
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MLA
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Valle, Giovanni, et al. “Synthesis and x-ray crystal structure of a tin(IV) tetrahalide adduct with a crown ether.” Inorganica Chimica Acta, vol. 82, no. 1, Feb. 1984, pp. 81-84. https://doi.org/10.1016/S0020-1693(00)82542-6.