Thermochimica Acta, volume 388, issue 1-2, pages 233-251

Thermal decomposition of aminotetrazoles

A.I. Lesnikovich ¹

Oleg A. Ivashkevich ¹

S.V. Levchik ¹

A.I. Balabanovich ¹

P.N. Gaponik ¹

A.A. Kulak ¹

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Research Institute for Physical Chemical Problems, Belarusian State University, Leningradskaya 14, Minsk 220050, Belarus |

Publication type: Journal Article

Publication date: 2002-06-01

Elsevier

Journal: Thermochimica Acta

Quartile SCImago

Quartile WOS

Impact factor: 3.5

ISSN: 00406031, 1872762X

DOI: 10.1016/S0040-6031(02)00027-8

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Physical and Theoretical Chemistry

Condensed Matter Physics

Instrumentation

Abstract

The thermal decomposition of 5-aminotetrazole (5-AT), 1-methyl-5-aminotetrazole (MAT), 1,5-diaminotetrazole (DAT), poly-1-vinyl-5-aminotetrazole (PVAT) and sodium salt of 5-aminotetrazole (SAT) have been studied by thermogravimetry, thermal volumetric analysis (TVA), DSC, DTA and evolved gas analysis (EGA). The kinetic parameters of the thermal decomposition of aminotetrazoles were calculated either by the Ozawa method or by the method of invariant kinetic parameters (IKP). The gaseous products, volatile condensed products and solid residues were identified by FTIR and gas chromatography–mass-spectrometry (GS/MS). The total energies and the energies of chemical bonds of various isomeric forms of 5-AT and MAT have been calculated ab initio using MP2/6-31G∗∗ theory level and MNDO approximation. Based on the content of products of thermal decomposition and the kinetic consideration, the mechanism of thermal decomposition of aminotetrazoles has been derived. Two routes of the splitting of tetrazole ring leading either to elimination nitrogen or hydrogen azide are suggested. The contribution of each route is changing upon the advancement of the process. It was assumed, that hydrogen azide splits out from the prothotropic forms of the tetrazole ring, which have hydrogen atoms by nitrogens in the ring. Experimental study as well as literature data on the amino-imino tautomerism are in agreement with the suggested mechanism of the decomposition of the tetrazole ring. It is shown that secondary reactions significantly extend variety of the products of thermal decomposition of aminotetrazoles.

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Lesnikovich A. et al. Thermal decomposition of aminotetrazoles // Thermochimica Acta. 2002. Vol. 388. No. 1-2. pp. 233-251.

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Lesnikovich A., Ivashkevich O. A., Levchik S., Balabanovich A., Gaponik P., Kulak A. Thermal decomposition of aminotetrazoles // Thermochimica Acta. 2002. Vol. 388. No. 1-2. pp. 233-251.

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TY - JOUR

DO - 10.1016/S0040-6031(02)00027-8

UR - https://doi.org/10.1016/S0040-6031(02)00027-8

TI - Thermal decomposition of aminotetrazoles

T2 - Thermochimica Acta

AU - Lesnikovich, A.I.

AU - Ivashkevich, Oleg A.

AU - Levchik, S.V.

AU - Balabanovich, A.I.

AU - Gaponik, P.N.

AU - Kulak, A.A.

PY - 2002

DA - 2002/06/01 00:00:00

PB - Elsevier

SP - 233-251

IS - 1-2

VL - 388

SN - 0040-6031

SN - 1872-762X

ER -

BibTex |

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BibTex Copy

@article{2002_Lesnikovich,

author = {A.I. Lesnikovich and Oleg A. Ivashkevich and S.V. Levchik and A.I. Balabanovich and P.N. Gaponik and A.A. Kulak},

title = {Thermal decomposition of aminotetrazoles},

journal = {Thermochimica Acta},

year = {2002},

volume = {388},

publisher = {Elsevier},

month = {jun},

url = {https://doi.org/10.1016/S0040-6031(02)00027-8},

number = {1-2},

pages = {233--251},

doi = {10.1016/S0040-6031(02)00027-8}

}

MLA

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MLA Copy

Lesnikovich, A.I., et al. “Thermal decomposition of aminotetrazoles.” Thermochimica Acta, vol. 388, no. 1-2, Jun. 2002, pp. 233-251. https://doi.org/10.1016/S0040-6031(02)00027-8.

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Publisher

Elsevier

Journal

Thermochimica Acta

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Impact factor

3.5

ISSN

00406031 (Print)
1872762X (Electronic)