Thin Solid Films, volume 359, issue 1, pages 55-60

Preparation and characterization of polymer thin films containing silver and silver sulfide nanoparticles

Kensuke Akamatsu

Kensuke Akamatsu ¹

Shodo Takei ²

Minoru Mizuhata

Minoru Mizuhata ²

Akihiko Kajinami ²

Shigehito Deki ²

Shinji Takeoka

Shinji Takeoka ³

Minoru Fujii

Minoru Fujii ⁴

Shinji Hayashi

Shinji Hayashi ⁴

KEIICHI YAMAMOTO ⁴

Hide authors affiliations Show authors affiliations: 4 affiliations

Division of Molecular Science, The Graduate School of Science and Technology, Kobe University, Rokkodai, Nada, Kobe 657-8501, Japan |

Department of Chemical Science and Engineering, Faculty of Engineering, Kobe University, Rokkodai, Nada, Kobe 657-8501, Japan |

Division of Mathematical and Material Science, The Graduate School of Science and Technology, Kobe University, Rokkodai, Nada, Kobe 657‐8501, Japan |

⁴

Department of Electrical and Electronics Engineering, Faculty of Engineering, Kobe University, Rokkodai, Nada, Kobe 657-8501, Japan |

Publication type: Journal Article

Publication date: 2000-01-01

Elsevier

Journal: Thin Solid Films

Quartile SCImago

Quartile WOS

Impact factor: 2.1

ISSN: 00406090

DOI: 10.1016/S0040-6090(99)00684-7

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Materials Chemistry

Metals and Alloys

Surfaces, Coatings and Films

Electronic, Optical and Magnetic Materials

Surfaces and Interfaces

Abstract

Composite thin films consisting of nano-sized Ag particles dispersed in nylon 11 thin films have been prepared by using a thermal relaxation technique. The films obtained were characterized by transmission electron microscopy (TEM), electron diffraction (ED), energy-dispersive X-ray (EDX) microanalysis, and optical absorption spectroscopy. The Ag nanoparticles with 4.5–9.1 nm in diameter were found to be isolated individually and dispersed uniformly in the nylon 11 matrix. The volume fraction and the mean size of Ag nanoparticles in the film could be controlled by varying the initial amount of Ag deposition. Optical absorption peak due to the surface plasmon resonance of the Ag particles were observed around 430 nm and shifted to a longer wavelength with increasing the mean size of Ag nanoparticles, and absorbance increased simultaneously. We have also prepared Ag 2 S nanoparticles with 4.7–11.2 nm in diameter in nylon 11 films from exposing the Ag/nylon 11 films to H 2 S/O 2 mixed gas. ED patterns of the particles formed after the reaction with H 2 S were completely indexed as those of β -Ag 2 S with a monoclinic structure. The onset of the optical absorption spectra is similar to that of bulk β -Ag 2 S, suggesting that Ag 2 S nanoparticles with diameter of ca. 5nm preserve the band structure of bulk Ag 2 S.

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Akamatsu K. et al. Preparation and characterization of polymer thin films containing silver and silver sulfide nanoparticles // Thin Solid Films. 2000. Vol. 359. No. 1. pp. 55-60.

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Akamatsu K., Akamatsu K., Takei S., Mizuhata M., Mizuhata M., Kajinami A., Deki S., Takeoka S., Takeoka S., Fujii M., Fujii M., Hayashi S., Hayashi S., YAMAMOTO K. Preparation and characterization of polymer thin films containing silver and silver sulfide nanoparticles // Thin Solid Films. 2000. Vol. 359. No. 1. pp. 55-60.

RIS |

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RIS Copy

TY - JOUR

DO - 10.1016/S0040-6090(99)00684-7

UR - https://doi.org/10.1016/S0040-6090(99)00684-7

TI - Preparation and characterization of polymer thin films containing silver and silver sulfide nanoparticles

T2 - Thin Solid Films

AU - Akamatsu, Kensuke

AU - Takei, Shodo

AU - Mizuhata, Minoru

AU - Kajinami, Akihiko

AU - Deki, Shigehito

AU - Takeoka, Shinji

AU - Fujii, Minoru

AU - Hayashi, Shinji

AU - YAMAMOTO, KEIICHI

AU - Akamatsu, Kensuke

AU - Mizuhata, Minoru

AU - Takeoka, Shinji

AU - Fujii, Minoru

AU - Hayashi, Shinji

PY - 2000

DA - 2000/01/01 00:00:00

PB - Elsevier

SP - 55-60

IS - 1

VL - 359

SN - 0040-6090

ER -

BibTex |

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@article{2000_Akamatsu,

author = {Kensuke Akamatsu and Shodo Takei and Minoru Mizuhata and Akihiko Kajinami and Shigehito Deki and Shinji Takeoka and Minoru Fujii and Shinji Hayashi and KEIICHI YAMAMOTO and Kensuke Akamatsu and Minoru Mizuhata and Shinji Takeoka and Minoru Fujii and Shinji Hayashi},

title = {Preparation and characterization of polymer thin films containing silver and silver sulfide nanoparticles},

journal = {Thin Solid Films},

year = {2000},

volume = {359},

publisher = {Elsevier},

month = {jan},

url = {https://doi.org/10.1016/S0040-6090(99)00684-7},

number = {1},

pages = {55--60},

doi = {10.1016/S0040-6090(99)00684-7}

}

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MLA Copy

Akamatsu, Kensuke, et al. “Preparation and characterization of polymer thin films containing silver and silver sulfide nanoparticles.” Thin Solid Films, vol. 359, no. 1, Jan. 2000, pp. 55-60. https://doi.org/10.1016/S0040-6090(99)00684-7.

Found error?

Publisher

Elsevier

Journal

Thin Solid Films

Quartile SCImago

Quartile WOS

Impact factor

2.1

ISSN

00406090 (Print)