Polyhedron

, том 18 , издание 8-9 , страницы 1159-1162

Synthesis and structure of the phosphinophosphide niobocene complex Cp2Nb(PPh2)(PHPh2)

Тип публикации: Journal Article

Дата публикации: 1999-03-01

Elsevier

Polyhedron

scimago Q3

wos Q2

БС2

SJR: 0.396

CiteScore: 4.9

Impact factor: 2.6

ISSN: 02775387, 18733719

DOI: 10.1016/S0277-5387(98)00408-2

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Materials Chemistry

Inorganic Chemistry

Physical and Theoretical Chemistry

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Abstract The phosphinophosphido niobocene complex Cp 2 Nb(PHPh 2 )(PPh 2 ) ( 2 ) was prepared by deprotonation of the cationic diphosphino complex [Cp 2 Nb(PHPh 2 ) 2 ]Cl ( 3 ). Complex 2 is thermally unstable and readily dissociates phosphine to give the ortho -metallated complex Cp 2 Nb(PHPhC 6 H 4 −). Crystal structure determination of 2 supported its formulation as the phosphinophosphido compound. The Nb–P(1) (phosphino) bond length is 2.524(2) A and Nb–P(2) (phosphido) bond length is 2.610(2) A.

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Nikonov G. I. et al. Synthesis and structure of the phosphinophosphide niobocene complex Cp2Nb(PPh2)(PHPh2) // Polyhedron. 1999. Vol. 18. No. 8-9. pp. 1159-1162.

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Nikonov G. I., Lemenovskii D. A., Dorogov K. Yu., Churakov A. V. Synthesis and structure of the phosphinophosphide niobocene complex Cp2Nb(PPh2)(PHPh2) // Polyhedron. 1999. Vol. 18. No. 8-9. pp. 1159-1162.

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TY - JOUR

DO - 10.1016/S0277-5387(98)00408-2

UR - https://linkinghub.elsevier.com/retrieve/pii/S0277538798004082

TI - Synthesis and structure of the phosphinophosphide niobocene complex Cp2Nb(PPh2)(PHPh2)

T2 - Polyhedron

AU - Nikonov, G. I.

AU - Lemenovskii, Dmitry A

AU - Dorogov, Konstantin Yu

AU - Churakov, Andrei V.

PY - 1999

DA - 1999/03/01

PB - Elsevier

SP - 1159-1162

IS - 8-9

VL - 18

SN - 0277-5387

SN - 1873-3719

ER -

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@article{1999_Nikonov,

author = {G. I. Nikonov and Dmitry A Lemenovskii and Konstantin Yu Dorogov and Andrei V. Churakov},

title = {Synthesis and structure of the phosphinophosphide niobocene complex Cp2Nb(PPh2)(PHPh2)},

journal = {Polyhedron},

year = {1999},

volume = {18},

publisher = {Elsevier},

month = {mar},

url = {https://linkinghub.elsevier.com/retrieve/pii/S0277538798004082},

number = {8-9},

pages = {1159--1162},

doi = {10.1016/S0277-5387(98)00408-2}

}

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Nikonov, G. I., et al. “Synthesis and structure of the phosphinophosphide niobocene complex Cp2Nb(PPh2)(PHPh2).” Polyhedron, vol. 18, no. 8-9, Mar. 1999, pp. 1159-1162. https://linkinghub.elsevier.com/retrieve/pii/S0277538798004082.