Synthesis and resolution of an α-phenyl substituted ortho-palladated matrix
Publication type: Journal Article
Publication date: 1999-08-01
Catalysis
Organic Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Abstract A novel ortho -palladated benzylaminate matrix bearing phenyl substituent at the α-carbon stereocenter was prepared in the racemic state by direct intramolecular palladation of tertiary diphenylmethylamine with palladium(II) acetate; its structure and palladacycle conformation were determined by 1 H NMR studies of the mononuclear triphenylphosphine adduct. The resolution of the dimeric complex was performed via recrystallization of its diastereomeric ( S )-prolinate derivatives. The absolute configuration ( R C , R C ) of the enantiopure dimer thus obtained was determined by an X-ray diffraction investigation of the less soluble ( R C , S C S N )-diastereomer of its ( S )-prolinate adduct.
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26
Total citations:
26
Citations from 2025:
1
(3.85%)
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MLA
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GOST
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Dunina V. V. et al. Synthesis and resolution of an α-phenyl substituted ortho-palladated matrix // Tetrahedron Asymmetry. 1999. Vol. 10. No. 16. pp. 3147-3155.
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Dunina V. V., Razmyslova E. D., Kuz'mina L. G., Churakov A. V., Rubina M. Yu., Grishin Y. K. Synthesis and resolution of an α-phenyl substituted ortho-palladated matrix // Tetrahedron Asymmetry. 1999. Vol. 10. No. 16. pp. 3147-3155.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1016/S0957-4166(99)00319-5
UR - https://linkinghub.elsevier.com/retrieve/pii/S0957416699003195
TI - Synthesis and resolution of an α-phenyl substituted ortho-palladated matrix
T2 - Tetrahedron Asymmetry
AU - Dunina, Valery V
AU - Razmyslova, Elena D.
AU - Kuz'mina, Lyudmila G.
AU - Churakov, Andrei V.
AU - Rubina, Marina Yu
AU - Grishin, Yurii K
PY - 1999
DA - 1999/08/01
PB - Elsevier
SP - 3147-3155
IS - 16
VL - 10
SN - 0957-4166
SN - 1362-511X
ER -
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BibTex (up to 50 authors)
Copy
@article{1999_Dunina,
author = {Valery V Dunina and Elena D. Razmyslova and Lyudmila G. Kuz'mina and Andrei V. Churakov and Marina Yu Rubina and Yurii K Grishin},
title = {Synthesis and resolution of an α-phenyl substituted ortho-palladated matrix},
journal = {Tetrahedron Asymmetry},
year = {1999},
volume = {10},
publisher = {Elsevier},
month = {aug},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0957416699003195},
number = {16},
pages = {3147--3155},
doi = {10.1016/S0957-4166(99)00319-5}
}
Cite this
MLA
Copy
Dunina, Valery V., et al. “Synthesis and resolution of an α-phenyl substituted ortho-palladated matrix.” Tetrahedron Asymmetry, vol. 10, no. 16, Aug. 1999, pp. 3147-3155. https://linkinghub.elsevier.com/retrieve/pii/S0957416699003195.
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