volume 114 pages 105128

Microwave-assisted rapid synthesis of spirooxindole-pyrrolizidine analogues and their activity as anti-amyloidogenic agents

Nilamuni H De Silva 1
Suneela Pyreddy 1
Ewan W. Blanch 1
Helmut M Hugel 1
Subashani Maniam 1
Publication typeJournal Article
Publication date2021-09-01
scimago Q1
wos Q1
SJR0.786
CiteScore8.3
Impact factor4.7
ISSN00452068, 10902120
Organic Chemistry
Drug Discovery
Biochemistry
Molecular Biology
Abstract
A library of Sox-pyrrolizidines was rapidly prepared by microwave-assisted, one-pot, three-component, 1,3-dipolar cycloaddition of azomethine ylides from l-proline and isatin, with various β-nitrostyrenes. Nitro-Sox compounds, 4b, 4d and 4e inhibit HEWL amyloid fibril formation by ThT studies with percentages of fluorescence intensity of 55.4, 42.9 and 40.3%, respectively. Further studies with MTT assay, Raman spectroscopy, TEM and molecular docking supported these promising candidates for activity against amyloid misfolding, a phenomenon leading to Alzheimer's disease pathology.
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GOST Copy
De Silva N. H. et al. Microwave-assisted rapid synthesis of spirooxindole-pyrrolizidine analogues and their activity as anti-amyloidogenic agents // Bioorganic Chemistry. 2021. Vol. 114. p. 105128.
GOST all authors (up to 50) Copy
De Silva N. H., Pyreddy S., Blanch E. W., Hugel H. M., Maniam S. Microwave-assisted rapid synthesis of spirooxindole-pyrrolizidine analogues and their activity as anti-amyloidogenic agents // Bioorganic Chemistry. 2021. Vol. 114. p. 105128.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1016/j.bioorg.2021.105128
UR - https://doi.org/10.1016/j.bioorg.2021.105128
TI - Microwave-assisted rapid synthesis of spirooxindole-pyrrolizidine analogues and their activity as anti-amyloidogenic agents
T2 - Bioorganic Chemistry
AU - De Silva, Nilamuni H
AU - Pyreddy, Suneela
AU - Blanch, Ewan W.
AU - Hugel, Helmut M
AU - Maniam, Subashani
PY - 2021
DA - 2021/09/01
PB - Elsevier
SP - 105128
VL - 114
PMID - 34225163
SN - 0045-2068
SN - 1090-2120
ER -
BibTex
Cite this
BibTex (up to 50 authors) Copy
@article{2021_De Silva,
author = {Nilamuni H De Silva and Suneela Pyreddy and Ewan W. Blanch and Helmut M Hugel and Subashani Maniam},
title = {Microwave-assisted rapid synthesis of spirooxindole-pyrrolizidine analogues and their activity as anti-amyloidogenic agents},
journal = {Bioorganic Chemistry},
year = {2021},
volume = {114},
publisher = {Elsevier},
month = {sep},
url = {https://doi.org/10.1016/j.bioorg.2021.105128},
pages = {105128},
doi = {10.1016/j.bioorg.2021.105128}
}