Carbon, volume 43, issue 8, pages 1731-1742

Raman microspectroscopy of soot and related carbonaceous materials: Spectral analysis and structural information

A. Sadezky ¹

H Muckenhuber ²

Hinrich Grothe ²

Reinhard Niessner ³

Ulrich Pöschl ⁴

Hide authors affiliations Show authors affiliations: 4 affiliations

Atmospheric Chemistry, Max Planck Institute for Chemistry, Max Planck Society |

Institute of Materials Chemistry, Vienna University of Technology, Veterinaerplatz 1/GA, A-1210 Vienna, Austria |

Institute of Hydrochemistry, Technical University of Munich, Marchioninistr. 17, D-81377, Munich, Germany |

⁴

Biogeochemistry, Max Planck Institute for Chemistry, Max Planck Society |

Publication type: Journal Article

Publication date: 2005-07-01

Elsevier

Journal: Carbon

Quartile SCImago

Quartile WOS

Impact factor: 10.9

ISSN: 00086223

DOI: 10.1016/j.carbon.2005.02.018

Copy DOI

General Chemistry

General Materials Science

Abstract

Abstract Experimental conditions and mathematical fitting procedures for the collection and analysis of Raman spectra of soot and related carbonaceous materials have been investigated and optimised with a Raman microscope system operated at three different laser excitation wavelengths (514, 633, and 780 nm). Several band combinations for spectral analysis have been tested, and a combination of four Lorentzian-shaped bands (G, D1, D2, D4) at about 1580, 1350, 1620, and 1200 cm −1 , respectively, with a Gaussian-shaped band (D3) at ∼1500 cm −1 was best suited for the first-order spectra. The second-order spectra were best fitted with Lorentzian-shaped bands at about 2450, 2700, 2900, and 3100 cm −1 . Spectral parameters (band positions, full widths at half maximum, and intensity ratios) are reported for several types of industrial carbon black (Degussa Printex, Cabot Monarch), diesel soot (particulate matter from modern heavy duty vehicle and passenger car engine exhaust, NIST SRM1650), spark-discharge soot (Palas GfG100), and graphite. Several parameters, in particular the width of the D1 band at ∼1350 cm −1 , provide structural information and allow to discriminate the sample materials, but the characterisation and distinction of different types of soot is limited by the experimental reproducibility of the spectra and the statistical uncertainties of curve fitting. The results are discussed and compared with X-ray diffraction measurements and earlier Raman spectroscopic studies of comparable materials, where different measurement and fitting procedures had been applied.

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Citations by journals

	20 40 60 80 100 120 140 160 180 200
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ACS applied materials & interfaces	ACS applied materials & interfaces, 65, 1.85% ACS applied materials & interfaces 65 publications, 1.85%
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Journal of Analytical and Applied Pyrolysis	Journal of Analytical and Applied Pyrolysis, 30, 0.85% Journal of Analytical and Applied Pyrolysis 30 publications, 0.85%
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ACS Applied Energy Materials	ACS Applied Energy Materials, 26, 0.74% ACS Applied Energy Materials 26 publications, 0.74%
Journal of Raman Spectroscopy	Journal of Raman Spectroscopy, 26, 0.74% Journal of Raman Spectroscopy 26 publications, 0.74%
Journal of the Electrochemical Society	Journal of the Electrochemical Society, 25, 0.71% Journal of the Electrochemical Society 25 publications, 0.71%
Nanomaterials	Nanomaterials, 25, 0.71% Nanomaterials 25 publications, 0.71%
Journal of Physical Chemistry C	Journal of Physical Chemistry C, 25, 0.71% Journal of Physical Chemistry C 25 publications, 0.71%
Ceramics International	Ceramics International, 24, 0.68% Ceramics International 24 publications, 0.68%
ACS Catalysis	ACS Catalysis, 24, 0.68% ACS Catalysis 24 publications, 0.68%
ChemElectroChem	ChemElectroChem, 24, 0.68% ChemElectroChem 24 publications, 0.68%
	20 40 60 80 100 120 140 160 180 200

Citations by publishers

	200 400 600 800 1000 1200 1400 1600 1800
Elsevier	Elsevier, 1683, 47.85% Elsevier 1683 publications, 47.85%
American Chemical Society (ACS)	American Chemical Society (ACS), 415, 11.8% American Chemical Society (ACS) 415 publications, 11.8%
Wiley	Wiley, 355, 10.09% Wiley 355 publications, 10.09%
Springer Nature	Springer Nature, 252, 7.17% Springer Nature 252 publications, 7.17%
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Taylor & Francis	Taylor & Francis, 46, 1.31% Taylor & Francis 46 publications, 1.31%
IOP Publishing	IOP Publishing, 41, 1.17% IOP Publishing 41 publications, 1.17%
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Pleiades Publishing	Pleiades Publishing, 25, 0.71% Pleiades Publishing 25 publications, 0.71%
Copernicus	Copernicus, 19, 0.54% Copernicus 19 publications, 0.54%
American Institute of Physics (AIP)	American Institute of Physics (AIP), 15, 0.43% American Institute of Physics (AIP) 15 publications, 0.43%
Frontiers Media S.A.	Frontiers Media S.A., 14, 0.4% Frontiers Media S.A. 14 publications, 0.4%
SAGE	SAGE, 12, 0.34% SAGE 12 publications, 0.34%
Trans Tech Publications	Trans Tech Publications, 10, 0.28% Trans Tech Publications 10 publications, 0.28%
SAE International	SAE International, 9, 0.26% SAE International 9 publications, 0.26%
Walter de Gruyter	Walter de Gruyter, 8, 0.23% Walter de Gruyter 8 publications, 0.23%
EDP Sciences	EDP Sciences, 7, 0.2% EDP Sciences 7 publications, 0.2%
Hindawi Limited	Hindawi Limited, 6, 0.17% Hindawi Limited 6 publications, 0.17%
World Scientific	World Scientific, 5, 0.14% World Scientific 5 publications, 0.14%
Iron and Steel Institute of Japan	Iron and Steel Institute of Japan, 5, 0.14% Iron and Steel Institute of Japan 5 publications, 0.14%
University of Science and Technology Beijing	University of Science and Technology Beijing, 5, 0.14% University of Science and Technology Beijing 5 publications, 0.14%
Optical Society of America	Optical Society of America, 5, 0.14% Optical Society of America 5 publications, 0.14%
American Association for the Advancement of Science (AAAS)	American Association for the Advancement of Science (AAAS), 4, 0.11% American Association for the Advancement of Science (AAAS) 4 publications, 0.11%
ASME	ASME, 4, 0.11% ASME 4 publications, 0.11%
Mary Ann Liebert	Mary Ann Liebert, 4, 0.11% Mary Ann Liebert 4 publications, 0.11%
IOS Press	IOS Press, 4, 0.11% IOS Press 4 publications, 0.11%
Japan Society of Applied Physics	Japan Society of Applied Physics, 4, 0.11% Japan Society of Applied Physics 4 publications, 0.11%
Electrochemical Science Group, University of Belgrade	Electrochemical Science Group, University of Belgrade, 4, 0.11% Electrochemical Science Group, University of Belgrade 4 publications, 0.11%
	200 400 600 800 1000 1200 1400 1600 1800

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Sadezky A. et al. Raman microspectroscopy of soot and related carbonaceous materials: Spectral analysis and structural information // Carbon. 2005. Vol. 43. No. 8. pp. 1731-1742.

GOST all authors (up to 50) Copy

Sadezky A., Muckenhuber H., Grothe H., Niessner R., Pöschl U. Raman microspectroscopy of soot and related carbonaceous materials: Spectral analysis and structural information // Carbon. 2005. Vol. 43. No. 8. pp. 1731-1742.

RIS |

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RIS Copy

TY - JOUR

DO - 10.1016/j.carbon.2005.02.018

UR - https://doi.org/10.1016/j.carbon.2005.02.018

TI - Raman microspectroscopy of soot and related carbonaceous materials: Spectral analysis and structural information

T2 - Carbon

AU - Sadezky, A.

AU - Muckenhuber, H

AU - Grothe, Hinrich

AU - Niessner, Reinhard

AU - Pöschl, Ulrich

PY - 2005

DA - 2005/07/01 00:00:00

PB - Elsevier

SP - 1731-1742

IS - 8

VL - 43

SN - 0008-6223

ER -

BibTex |

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BibTex Copy

@article{2005_Sadezky,

author = {A. Sadezky and H Muckenhuber and Hinrich Grothe and Reinhard Niessner and Ulrich Pöschl},

title = {Raman microspectroscopy of soot and related carbonaceous materials: Spectral analysis and structural information},

journal = {Carbon},

year = {2005},

volume = {43},

publisher = {Elsevier},

month = {jul},

url = {https://doi.org/10.1016/j.carbon.2005.02.018},

number = {8},

pages = {1731--1742},

doi = {10.1016/j.carbon.2005.02.018}

}

MLA

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MLA Copy

Sadezky, A., et al. “Raman microspectroscopy of soot and related carbonaceous materials: Spectral analysis and structural information.” Carbon, vol. 43, no. 8, Jul. 2005, pp. 1731-1742. https://doi.org/10.1016/j.carbon.2005.02.018.

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Publisher

Elsevier

Journal

Carbon

Quartile SCImago

Quartile WOS

Impact factor

10.9

ISSN

00086223 (Print)