The formation of a peroxoantimonate thin film coating on graphene oxide (GO) and the influence of the GO on its transformation to antimony oxides and elemental antimony
Publication type: Journal Article
Publication date: 2012-12-01
scimago Q1
wos Q1
SJR: 2.320
CiteScore: 21.4
Impact factor: 11.6
ISSN: 00086223, 18733891
General Chemistry
General Materials Science
Abstract
Abstract The ultrathin peroxoantimonate coating of graphene oxide from hydrogen peroxide-rich solutions of hydroxoantimonate is demonstrated. An amorphous 1–2 nm Sb (V) oxide film is formed and can be further crystallized by exposure to an electron beam to give a 2–5 nm thick supported Sb 6 O 13 particulate coating. Heat treatment of the peroxoantimonate yielded different crystalline oxides, whereas in the presence of the graphene support only trigonal Sb (0) was produced by heat treatment in vacuum or an argon atmosphere. The graphene oxide support is essential for the formation of the Sb (0) phase and even in air a substantial elemental antimony was obtained. Whereas heat treatment of uncoated graphene oxide in an inert atmosphere produces reduced graphene oxide, the antimony oxide coated graphene oxide is not reduced by the heat treatment. Only after the supported antimony oxide is reduced to give the trigonal Sb (0) phase the graphene oxide was reduced by the heat treatment. The phases before and after the different heat treatments are characterized by electron and X-ray diffraction, thermal analysis, XPS studies, electron microscopy and wet chemistry.
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Total citations:
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Citations from 2025:
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GOST
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Sladkevich S. et al. The formation of a peroxoantimonate thin film coating on graphene oxide (GO) and the influence of the GO on its transformation to antimony oxides and elemental antimony // Carbon. 2012. Vol. 50. No. 15. pp. 5463-5471.
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Sladkevich S., Gun J., Prikhodchenko P. V., Gutkin V., Mikhaylov A., Medvedev A. S., Tripolskaya T. A., Lev O. The formation of a peroxoantimonate thin film coating on graphene oxide (GO) and the influence of the GO on its transformation to antimony oxides and elemental antimony // Carbon. 2012. Vol. 50. No. 15. pp. 5463-5471.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1016/j.carbon.2012.07.033
UR - https://doi.org/10.1016/j.carbon.2012.07.033
TI - The formation of a peroxoantimonate thin film coating on graphene oxide (GO) and the influence of the GO on its transformation to antimony oxides and elemental antimony
T2 - Carbon
AU - Sladkevich, Sergey
AU - Gun, Jenny
AU - Prikhodchenko, Petr V.
AU - Gutkin, Vitaly
AU - Mikhaylov, Alexey
AU - Medvedev, Alexander S.
AU - Tripolskaya, Tatiana A
AU - Lev, Ovadia
PY - 2012
DA - 2012/12/01
PB - Elsevier
SP - 5463-5471
IS - 15
VL - 50
SN - 0008-6223
SN - 1873-3891
ER -
Cite this
BibTex (up to 50 authors)
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@article{2012_Sladkevich,
author = {Sergey Sladkevich and Jenny Gun and Petr V. Prikhodchenko and Vitaly Gutkin and Alexey Mikhaylov and Alexander S. Medvedev and Tatiana A Tripolskaya and Ovadia Lev},
title = {The formation of a peroxoantimonate thin film coating on graphene oxide (GO) and the influence of the GO on its transformation to antimony oxides and elemental antimony},
journal = {Carbon},
year = {2012},
volume = {50},
publisher = {Elsevier},
month = {dec},
url = {https://doi.org/10.1016/j.carbon.2012.07.033},
number = {15},
pages = {5463--5471},
doi = {10.1016/j.carbon.2012.07.033}
}
Cite this
MLA
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Sladkevich, Sergey, et al. “The formation of a peroxoantimonate thin film coating on graphene oxide (GO) and the influence of the GO on its transformation to antimony oxides and elemental antimony.” Carbon, vol. 50, no. 15, Dec. 2012, pp. 5463-5471. https://doi.org/10.1016/j.carbon.2012.07.033.