Carbohydrate Polymers, volume 94, issue 1, pages 505-510
A novel and simple procedure to synthesize chitosan-graft-polycaprolactone in an ionic liquid
Zhaodong Wang
1
,
Liuchun Zheng
2
,
Chuncheng Li
2
,
Dong Zhang
2
,
Yaonan Xiao
2
,
Guohu Guan
2
,
Wenxiang Zhu
2
Publication type: Journal Article
Publication date: 2013-04-01
Journal:
Carbohydrate Polymers
Quartile SCImago
Q1
Quartile WOS
Q1
Impact factor: 11.2
ISSN: 01448617, 18791344
Materials Chemistry
Organic Chemistry
Polymers and Plastics
Abstract
An ionic liquid, 1-ethyl-3-methylimidazolium acetate (EMIMAc), was synthesized and employed as a homogeneous and green reaction media to prepare chitosan-graft-polycaprolactone (CS-g-PCL) via ring-opening polymerization, using stannous octoate (Sn(Oct)2) as a catalyst. The structures and compositions of copolymers could be facilely controlled by the reaction conditions and feed ratios. The grafting content of polycaprolactone (PCL) could reach as high as 630%. The chemical structures of the copolymers were systematically characterized by (1)H NMR, Fourier transform infrared spectroscopy (FTIR) and wide-angle X-ray diffraction (WAXD), while thermal properties were studied by thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC). The thermal stability and glass transition temperature (Tg) of the graft copolymers vary regularly with the change of PCL grafting content.
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Citations by publishers
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5 publications, 7.94%
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Springer Nature
3 publications, 4.76%
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1 publication, 1.59%
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Thieme
1 publication, 1.59%
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Scientific Publishers
1 publication, 1.59%
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Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii
1 publication, 1.59%
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5
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25
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- We do not take into account publications without a DOI.
- Statistics recalculated only for publications connected to researchers, organizations and labs registered on the platform.
- Statistics recalculated weekly.
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Wang Z. et al. A novel and simple procedure to synthesize chitosan-graft-polycaprolactone in an ionic liquid // Carbohydrate Polymers. 2013. Vol. 94. No. 1. pp. 505-510.
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Wang Z., Zheng L., Li C., Zhang D., Xiao Y., Guan G., Zhu W. A novel and simple procedure to synthesize chitosan-graft-polycaprolactone in an ionic liquid // Carbohydrate Polymers. 2013. Vol. 94. No. 1. pp. 505-510.
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TY - JOUR
DO - 10.1016/j.carbpol.2013.01.090
UR - https://doi.org/10.1016/j.carbpol.2013.01.090
TI - A novel and simple procedure to synthesize chitosan-graft-polycaprolactone in an ionic liquid
T2 - Carbohydrate Polymers
AU - Wang, Zhaodong
AU - Zheng, Liuchun
AU - Li, Chuncheng
AU - Zhang, Dong
AU - Xiao, Yaonan
AU - Guan, Guohu
AU - Zhu, Wenxiang
PY - 2013
DA - 2013/04/01 00:00:00
PB - Elsevier
SP - 505-510
IS - 1
VL - 94
SN - 0144-8617
SN - 1879-1344
ER -
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@article{2013_Wang,
author = {Zhaodong Wang and Liuchun Zheng and Chuncheng Li and Dong Zhang and Yaonan Xiao and Guohu Guan and Wenxiang Zhu},
title = {A novel and simple procedure to synthesize chitosan-graft-polycaprolactone in an ionic liquid},
journal = {Carbohydrate Polymers},
year = {2013},
volume = {94},
publisher = {Elsevier},
month = {apr},
url = {https://doi.org/10.1016/j.carbpol.2013.01.090},
number = {1},
pages = {505--510},
doi = {10.1016/j.carbpol.2013.01.090}
}
Cite this
MLA
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Wang, Zhaodong, et al. “A novel and simple procedure to synthesize chitosan-graft-polycaprolactone in an ionic liquid.” Carbohydrate Polymers, vol. 94, no. 1, Apr. 2013, pp. 505-510. https://doi.org/10.1016/j.carbpol.2013.01.090.