Control of microwave-generated hot spots. Part IV. Control of hot spots on a heterogeneous microwave-absorber catalyst surface by a hybrid internal/external heating method
Publication type: Journal Article
Publication date: 2013-07-01
scimago Q1
wos Q2
SJR: 0.794
CiteScore: 7.9
Impact factor: 3.9
ISSN: 02552701, 18733204
General Chemistry
General Chemical Engineering
Process Chemistry and Technology
Industrial and Manufacturing Engineering
Energy Engineering and Power Technology
Abstract
A problem with microwave-absorbing heterogeneous catalysts (MAHCs) in non-polar solvents is resolved with a novel approach that also uses an external heating bath in combination with microwave heating. In non-polar solvents, the microwave radiation dielectrically and selectively heats only the catalyst resulting in the frequent occurrence of hot spots under these conditions. However, such hot spots can be controlled through a combined (hybrid) internal/external heating methodology (MAHS). Moreover, high temperatures can be maintained with significant energy saving. The potential benefit of MAHS has been examined by carrying out the synthesis of 4-methylbiphenyl using the Suzuki–Miyaura coupling reaction in toluene solvent in the presence of palladium catalytic particles supported on activated carbon particulates (Pd/AC). The hybrid internal/external heating method saved 65% of microwave energy and increased the chemical yield of 4-methylbiphenyl nearly twofold in comparison with a conventional microwave heating method.
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Horikoshi S. et al. Control of microwave-generated hot spots. Part IV. Control of hot spots on a heterogeneous microwave-absorber catalyst surface by a hybrid internal/external heating method // Chemical Engineering and Processing: Process Intensification. 2013. Vol. 69. pp. 52-56.
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Horikoshi S., Osawa A., Sakamoto S., Serpone N. Control of microwave-generated hot spots. Part IV. Control of hot spots on a heterogeneous microwave-absorber catalyst surface by a hybrid internal/external heating method // Chemical Engineering and Processing: Process Intensification. 2013. Vol. 69. pp. 52-56.
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TY - JOUR
DO - 10.1016/j.cep.2013.02.003
UR - https://doi.org/10.1016/j.cep.2013.02.003
TI - Control of microwave-generated hot spots. Part IV. Control of hot spots on a heterogeneous microwave-absorber catalyst surface by a hybrid internal/external heating method
T2 - Chemical Engineering and Processing: Process Intensification
AU - Horikoshi, Satoshi
AU - Osawa, Atsushi
AU - Sakamoto, Shintaro
AU - Serpone, Nick
PY - 2013
DA - 2013/07/01
PB - Elsevier
SP - 52-56
VL - 69
SN - 0255-2701
SN - 1873-3204
ER -
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@article{2013_Horikoshi,
author = {Satoshi Horikoshi and Atsushi Osawa and Shintaro Sakamoto and Nick Serpone},
title = {Control of microwave-generated hot spots. Part IV. Control of hot spots on a heterogeneous microwave-absorber catalyst surface by a hybrid internal/external heating method},
journal = {Chemical Engineering and Processing: Process Intensification},
year = {2013},
volume = {69},
publisher = {Elsevier},
month = {jul},
url = {https://doi.org/10.1016/j.cep.2013.02.003},
pages = {52--56},
doi = {10.1016/j.cep.2013.02.003}
}