Ceramics International, volume 45, issue 12, pages 14991-14996

Overcoming the abnormal grain growth in Ga-doped Li7La3Zr2O12 to enhance the electrochemical stability against Li metal

Jianmeng Su ¹

Xiao Huang ¹

Zhen Song ²

Tongping Xiu ³

Michael E Badding ²

Jun Jin

Jun Jin ¹

Z. Wen ¹

Zhaoyin Wen

Hide authors affiliations Show authors affiliations: 3 affiliations

Center of Materials Science and Optoelectronics Engineering, University of Chinese Academy of Sciences, Beijing, 100049, China |

Corning Incorporated, Corning, NY 14831( USA) |

Corning Research Center China, Shanghai, 201206, China |

Publication type: Journal Article

Publication date: 2019-08-01

Elsevier

Journal: Ceramics International

Quartile SCImago

Quartile WOS

Impact factor: 5.2

ISSN: 02728842

DOI: 10.1016/j.ceramint.2019.04.236

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Materials Chemistry

Surfaces, Coatings and Films

Ceramics and Composites

Electronic, Optical and Magnetic Materials

Process Chemistry and Technology

Abstract

Li 7 La 3 Zr 2 O 12 (LLZO) solid electrolyte is a promising candidate for next generation batteries. In the LLZO family with various doping elements, Ga-doped LLZO (Ga-LLZO) delivers the highest Li-ion conductivity of higher than 1 × 10 −3  S cm −1 . However, Ga-LLZO ceramics always contain lots of overgrown huge grains after sintering, resulting in short-circuiting as applied with Li anode in batteries. Hence a simple two-step sintering strategy is developed to prepare fine-grained Ga-LLZO ceramics with good electrochemical properties. Pellets with the composition of Li 6.4 Ga 0.2 La 3 Zr 2 O 12 deliver pure garnet phase, uniform fine grains, high relative density of 97.3% and conductivity of 1.24 × 10 −3  S cm −1  at 27 °C after sintering at 1150 °C for 1 min and 1000 °C for 3 h. In addition, those fine-grained Ga-LLZO exhibit improved stability against molten Li. The Li/Ga-LLZO/Li symmetric cells show a critical current density of 0.7 mA cm −2 , and a stable cycling of over 600 h at 0.4 mA cm −2  at 27 °C. The Li/Ga-LLZO/LiFePO 4 full cells deliver reversible capacity of 150 mAh g −1 , showing negligible decay after 50 cycles. These results bring the Ga-LLZO electrolytes one step closer to practical application in solid-state batteries.

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Journal of Energy Storage	Journal of Energy Storage, 4, 4.35% Journal of Energy Storage 4 publications, 4.35%
Journal of Materials Chemistry A	Journal of Materials Chemistry A, 4, 4.35% Journal of Materials Chemistry A 4 publications, 4.35%
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Journal of the European Ceramic Society	Journal of the European Ceramic Society, 3, 3.26% Journal of the European Ceramic Society 3 publications, 3.26%
ACS Applied Energy Materials	ACS Applied Energy Materials, 3, 3.26% ACS Applied Energy Materials 3 publications, 3.26%
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Sustainable Energy and Fuels	Sustainable Energy and Fuels, 2, 2.17% Sustainable Energy and Fuels 2 publications, 2.17%
Small	Small, 2, 2.17% Small 2 publications, 2.17%
ACS Energy Letters	ACS Energy Letters, 1, 1.09% ACS Energy Letters 1 publication, 1.09%
Materials Science and Technology	Materials Science and Technology, 1, 1.09% Materials Science and Technology 1 publication, 1.09%
Journal of the Electrochemical Society	Journal of the Electrochemical Society, 1, 1.09% Journal of the Electrochemical Society 1 publication, 1.09%
Ionics	Ionics, 1, 1.09% Ionics 1 publication, 1.09%
Integrating Materials and Manufacturing Innovation	Integrating Materials and Manufacturing Innovation, 1, 1.09% Integrating Materials and Manufacturing Innovation 1 publication, 1.09%
Journal of Electronic Materials	Journal of Electronic Materials, 1, 1.09% Journal of Electronic Materials 1 publication, 1.09%
Nano Research	Nano Research, 1, 1.09% Nano Research 1 publication, 1.09%
Journal of Materials Science: Materials in Electronics	Journal of Materials Science: Materials in Electronics, 1, 1.09% Journal of Materials Science: Materials in Electronics 1 publication, 1.09%
Chinese Journal of Chemical Engineering	Chinese Journal of Chemical Engineering, 1, 1.09% Chinese Journal of Chemical Engineering 1 publication, 1.09%
Materials Chemistry and Physics	Materials Chemistry and Physics, 1, 1.09% Materials Chemistry and Physics 1 publication, 1.09%
Physics Open	Physics Open, 1, 1.09% Physics Open 1 publication, 1.09%
Journal of Materiomics	Journal of Materiomics, 1, 1.09% Journal of Materiomics 1 publication, 1.09%
Electrochimica Acta	Electrochimica Acta, 1, 1.09% Electrochimica Acta 1 publication, 1.09%
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Citations by publishers

	5 10 15 20 25 30 35
Elsevier	Elsevier, 35, 38.04% Elsevier 35 publications, 38.04%
Wiley	Wiley, 14, 15.22% Wiley 14 publications, 15.22%
American Chemical Society (ACS)	American Chemical Society (ACS), 14, 15.22% American Chemical Society (ACS) 14 publications, 15.22%
Royal Society of Chemistry (RSC)	Royal Society of Chemistry (RSC), 8, 8.7% Royal Society of Chemistry (RSC) 8 publications, 8.7%
Springer Nature	Springer Nature, 6, 6.52% Springer Nature 6 publications, 6.52%
Multidisciplinary Digital Publishing Institute (MDPI)	Multidisciplinary Digital Publishing Institute (MDPI), 3, 3.26% Multidisciplinary Digital Publishing Institute (MDPI) 3 publications, 3.26%
Nonferrous Metals Society of China	Nonferrous Metals Society of China, 2, 2.17% Nonferrous Metals Society of China 2 publications, 2.17%
Taylor & Francis	Taylor & Francis, 1, 1.09% Taylor & Francis 1 publication, 1.09%
The Electrochemical Society	The Electrochemical Society, 1, 1.09% The Electrochemical Society 1 publication, 1.09%
Chemical Industry Press	Chemical Industry Press, 1, 1.09% Chemical Industry Press 1 publication, 1.09%
Chinese Ceramic Society	Chinese Ceramic Society, 1, 1.09% Chinese Ceramic Society 1 publication, 1.09%
Institute of Research and Community Services Diponegoro University (LPPM UNDIP)	Institute of Research and Community Services Diponegoro University (LPPM UNDIP), 1, 1.09% Institute of Research and Community Services Diponegoro University (LPPM UNDIP) 1 publication, 1.09%
American Institute of Physics (AIP)	American Institute of Physics (AIP), 1, 1.09% American Institute of Physics (AIP) 1 publication, 1.09%
Hindawi Limited	Hindawi Limited, 1, 1.09% Hindawi Limited 1 publication, 1.09%
Higher Education Press	Higher Education Press, 1, 1.09% Higher Education Press 1 publication, 1.09%
IOP Publishing	IOP Publishing, 1, 1.09% IOP Publishing 1 publication, 1.09%
Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii	Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii, 1, 1.09% Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii 1 publication, 1.09%
	5 10 15 20 25 30 35

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Su J. et al. Overcoming the abnormal grain growth in Ga-doped Li7La3Zr2O12 to enhance the electrochemical stability against Li metal // Ceramics International. 2019. Vol. 45. No. 12. pp. 14991-14996.

GOST all authors (up to 50) Copy

Su J., Huang X., Song Z., Xiu T., Badding M. E., Jin J., Jin J., Wen Z., Wen Z. Overcoming the abnormal grain growth in Ga-doped Li7La3Zr2O12 to enhance the electrochemical stability against Li metal // Ceramics International. 2019. Vol. 45. No. 12. pp. 14991-14996.

RIS |

Cite this

RIS Copy

TY - JOUR

DO - 10.1016/j.ceramint.2019.04.236

UR - https://doi.org/10.1016/j.ceramint.2019.04.236

TI - Overcoming the abnormal grain growth in Ga-doped Li7La3Zr2O12 to enhance the electrochemical stability against Li metal

T2 - Ceramics International

AU - Su, Jianmeng

AU - Huang, Xiao

AU - Song, Zhen

AU - Xiu, Tongping

AU - Badding, Michael E

AU - Jin, Jun

AU - Wen, Zhaoyin

AU - Jin, Jun

AU - Wen, Z.

PY - 2019

DA - 2019/08/01 00:00:00

PB - Elsevier

SP - 14991-14996

IS - 12

VL - 45

SN - 0272-8842

ER -

BibTex |

Cite this

BibTex Copy

@article{2019_Su,

author = {Jianmeng Su and Xiao Huang and Zhen Song and Tongping Xiu and Michael E Badding and Jun Jin and Zhaoyin Wen and Jun Jin and Z. Wen},

title = {Overcoming the abnormal grain growth in Ga-doped Li7La3Zr2O12 to enhance the electrochemical stability against Li metal},

journal = {Ceramics International},

year = {2019},

volume = {45},

publisher = {Elsevier},

month = {aug},

url = {https://doi.org/10.1016/j.ceramint.2019.04.236},

number = {12},

pages = {14991--14996},

doi = {10.1016/j.ceramint.2019.04.236}

}

MLA

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Su, Jianmeng, et al. “Overcoming the abnormal grain growth in Ga-doped Li7La3Zr2O12 to enhance the electrochemical stability against Li metal.” Ceramics International, vol. 45, no. 12, Aug. 2019, pp. 14991-14996. https://doi.org/10.1016/j.ceramint.2019.04.236.

Found error?

Publisher

Elsevier

Journal

Ceramics International

Quartile SCImago

Quartile WOS

Impact factor

5.2

ISSN

02728842 (Print)