The novel calix[4]resorcinarene-PEG conjugate: Synthesis, self-association and encapsulation properties
Alina M Ermakova
1
,
Julia Morozova
1
,
Yana V Shalaeva
1
,
Alina Saifina
2
,
Olga B Bazanova
2
,
Anastasia S Sapunova
2
,
A. D. Voloshina
2
,
I. R. Nizameev
2, 3
,
M K Kadirov
2
,
Alexander I Konovalov
2
Publication type: Journal Article
Publication date: 2019-06-01
scimago Q1
wos Q2
SJR: 0.944
CiteScore: 9.6
Impact factor: 5.4
ISSN: 09277757, 18734359
Colloid and Surface Chemistry
Abstract
The synthesis and study of self-association and encapsulation ability of new low toxic conjugate of tetraphenyleneoxypentylcalix[4]resorcinarene and methoxy-poly(ethylene glycole) (C5OPh-mPEG) were described. The conjugate is characterized by 1H, 13C NMR, FT-IR, MS, SLS methods. In an aqueous solution the conjugate form multimicellar nanoparticles with low polydispersity value (0.1, DLS method). The self-association of the conjugate was studied by DLS, fluorescence, fluorescence anisotropy method, TEM, and SAXS methods. The SAXS data were detailed analyzed, and the conjugate associates structure as ellipsoidal core-shell particles was proposed. The encapsulation efficiency is a result of the affinity of the conjugate low rim substituents to substrates and reaches of 39.8, 26.7, and 28.9% toward naproxen, ibuprofen and doxorubicin drugs, respectively.
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Total citations:
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Citations from 2024:
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Ermakova A. M. et al. The novel calix[4]resorcinarene-PEG conjugate: Synthesis, self-association and encapsulation properties // Colloids and Surfaces A: Physicochemical and Engineering Aspects. 2019. Vol. 570. pp. 182-190.
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Ermakova A. M., Morozova J., Shalaeva Y. V., Gubaidullin A. T., Saifina A., Syakaev V. V., Bazanova O. B., Sapunova A. S., Voloshina A. D., Nizameev I. R., Kadirov M. K., Konovalov A. I. The novel calix[4]resorcinarene-PEG conjugate: Synthesis, self-association and encapsulation properties // Colloids and Surfaces A: Physicochemical and Engineering Aspects. 2019. Vol. 570. pp. 182-190.
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TY - JOUR
DO - 10.1016/j.colsurfa.2019.03.021
UR - https://doi.org/10.1016/j.colsurfa.2019.03.021
TI - The novel calix[4]resorcinarene-PEG conjugate: Synthesis, self-association and encapsulation properties
T2 - Colloids and Surfaces A: Physicochemical and Engineering Aspects
AU - Ermakova, Alina M
AU - Morozova, Julia
AU - Shalaeva, Yana V
AU - Gubaidullin, Aidar T.
AU - Saifina, Alina
AU - Syakaev, Victor V.
AU - Bazanova, Olga B
AU - Sapunova, Anastasia S
AU - Voloshina, A. D.
AU - Nizameev, I. R.
AU - Kadirov, M K
AU - Konovalov, Alexander I
PY - 2019
DA - 2019/06/01
PB - Elsevier
SP - 182-190
VL - 570
SN - 0927-7757
SN - 1873-4359
ER -
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BibTex (up to 50 authors)
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@article{2019_Ermakova,
author = {Alina M Ermakova and Julia Morozova and Yana V Shalaeva and Aidar T. Gubaidullin and Alina Saifina and Victor V. Syakaev and Olga B Bazanova and Anastasia S Sapunova and A. D. Voloshina and I. R. Nizameev and M K Kadirov and Alexander I Konovalov},
title = {The novel calix[4]resorcinarene-PEG conjugate: Synthesis, self-association and encapsulation properties},
journal = {Colloids and Surfaces A: Physicochemical and Engineering Aspects},
year = {2019},
volume = {570},
publisher = {Elsevier},
month = {jun},
url = {https://doi.org/10.1016/j.colsurfa.2019.03.021},
pages = {182--190},
doi = {10.1016/j.colsurfa.2019.03.021}
}