Electrochimica Acta, volume 296, pages 823-829

Synergistic regulation of garnet-type Ta-doped Li7La3Zr2O12 solid electrolyte by Li+ concentration and Li+ transport channel size

Yanhua Zhang ¹

Jiadong Deng ²

Dongwei Hu ³

Fei Chen ⁴

Qiang Shen ⁴

Jian Zhang ⁴

Shijie Dong ³

Hide authors affiliations Show authors affiliations: 4 affiliations

Hubei Provincial Key Laboratory of Green Materials for Light Industry, Hubei University of Technology, Wuhan, 430068, China |

School of Automotive Engineering,Wuhan University of Technology,Wuhan 430070, China) |

Hubei Provincial Key Laboratory of Green Materials for Light Industry Hubei University of Technology Wuhan 430068 China |

⁴

State Key Lab of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan 430070, China) |

Publication type: Journal Article

Publication date: 2019-02-01

Elsevier

Journal: Electrochimica Acta

Quartile SCImago

Quartile WOS

Impact factor: 6.6

ISSN: 00134686

DOI: 10.1016/j.electacta.2018.11.136

Copy DOI

General Chemical Engineering

Electrochemistry

Abstract

The Li+ concentration and Li+ transport channel size of garnet-type solid electrolyte Li7La3Zr2O12 are the two key factors associated with the improvement of Li ionic conductivity. Through precise control of the Li+ concentration and the Li+ transport channel size by Ta-doping (Li7-XLa3Zr2-XTaXO12, X = 0.2–1.0), synergistic regulation of the two factors is achieved. Results show that the optimum Li+ concentration seems to be at about 6.31 where the Li+ occupancy in LiO6 is high and the Li+ arrangement in LiO4 is disordering. With the Li+ concentration higher than 6.31, the occupancy in LiO4 sites remains constant but the Li+ arrangement in LiO4 becomes more and more ordering. At higher Li+ concentration of 6.52, Li+ arrangement becomes certain of ordering which should have reduced the grain conductivity, however, the grain conductivity is still as high as 9.84 × 10−4 S cm−1. This indicates that LLZO with this Li+ concentration have favorable Li+ transport channel size. The optimum Li+ transport channel size is about 12.95 ± 0.01 A. At Li+ concentration of 6.31, the proper Li+ concentration is the main factor for the high grain ionic conductivity of 10.1 × 10−4 S cm−1. While at Li+ concentration of 6.52, the suitable Li+ transport channel size is the main factor for the high grain ionic conductivity. In conclusion, the high grain ionic conductivity at Li+ concentration of 6.31–6.52 is due to the synergistic regulation of Li+ concentration and Li+ transport channel size.

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Zhang Y. et al. Synergistic regulation of garnet-type Ta-doped Li7La3Zr2O12 solid electrolyte by Li+ concentration and Li+ transport channel size // Electrochimica Acta. 2019. Vol. 296. pp. 823-829.

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Zhang Y., Deng J., Hu D., Chen F., Shen Q., Zhang J., Dong S. Synergistic regulation of garnet-type Ta-doped Li7La3Zr2O12 solid electrolyte by Li+ concentration and Li+ transport channel size // Electrochimica Acta. 2019. Vol. 296. pp. 823-829.

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RIS Copy

TY - JOUR

DO - 10.1016/j.electacta.2018.11.136

UR - https://doi.org/10.1016/j.electacta.2018.11.136

TI - Synergistic regulation of garnet-type Ta-doped Li7La3Zr2O12 solid electrolyte by Li+ concentration and Li+ transport channel size

T2 - Electrochimica Acta

AU - Zhang, Yanhua

AU - Deng, Jiadong

AU - Hu, Dongwei

AU - Chen, Fei

AU - Shen, Qiang

AU - Zhang, Jian

AU - Dong, Shijie

PY - 2019

DA - 2019/02/01 00:00:00

PB - Elsevier

SP - 823-829

VL - 296

SN - 0013-4686

ER -

BibTex

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BibTex Copy

@article{2019_Zhang,

author = {Yanhua Zhang and Jiadong Deng and Dongwei Hu and Fei Chen and Qiang Shen and Jian Zhang and Shijie Dong},

title = {Synergistic regulation of garnet-type Ta-doped Li7La3Zr2O12 solid electrolyte by Li+ concentration and Li+ transport channel size},

journal = {Electrochimica Acta},

year = {2019},

volume = {296},

publisher = {Elsevier},

month = {feb},

url = {https://doi.org/10.1016/j.electacta.2018.11.136},

pages = {823--829},

doi = {10.1016/j.electacta.2018.11.136}

}

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Elsevier

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Electrochimica Acta

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00134686 (Print)