Synthesis, crystal structure and characterization of alkali metal hydroxoantimonates
Alexey Mikhaylov
1
,
E A Melnik
1
,
Vladimir M. Novotortsev
1
,
Judith A. Howard
2
,
Jenny Gun
3
,
Subramanian Bharathi
3
,
Ovadia Lev
3
,
Publication type: Journal Article
Publication date: 2011-11-01
scimago Q3
wos Q2
SJR: 0.393
CiteScore: 5.5
Impact factor: 3.2
ISSN: 00201693, 18733255
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Abstract Several alkali metal hydroxoantimonates, K 2 [Sb(O)(OH) 5 ], Na[Sb(OH) 6 ], Cs[Sb(OH) 6 ] and Cs 2 [Sb 2 (μ-O) 2 (OH) 8 ] were isolated from aqueous solutions and characterized by single crystal and powder X-ray diffraction studies and by FTIR and thermal analysis. Crystal structures involving [Sb(O)(OH) 5 ] 2− were never anticipated before, and this is also the first disclosure of a dinuclear antimonate [Sb 2 (μ-O) 2 (OH) 8 ] 2− . Aqueous antimonate solutions of different pH were studied by high resolution electrospray mass spectrometry showing pH indifferent spectra and predominance of the mono and dinuclear antimonate species at pH 4–10.
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8
Total citations:
8
Citations from 2024:
1
(12%)
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GOST
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Mikhaylov A. et al. Synthesis, crystal structure and characterization of alkali metal hydroxoantimonates // Inorganica Chimica Acta. 2011. Vol. 378. No. 1. pp. 24-29.
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Mikhaylov A., Melnik E. A., Churakov A. V., Novotortsev V. M., Howard J. A., Sladkevich S., Gun J., Bharathi S., Lev O., Prikhodchenko P. V. Synthesis, crystal structure and characterization of alkali metal hydroxoantimonates // Inorganica Chimica Acta. 2011. Vol. 378. No. 1. pp. 24-29.
Cite this
RIS
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TY - JOUR
DO - 10.1016/j.ica.2011.08.007
UR - https://linkinghub.elsevier.com/retrieve/pii/S0020169311006499
TI - Synthesis, crystal structure and characterization of alkali metal hydroxoantimonates
T2 - Inorganica Chimica Acta
AU - Mikhaylov, Alexey
AU - Melnik, E A
AU - Churakov, Andrei V.
AU - Novotortsev, Vladimir M.
AU - Howard, Judith A.
AU - Sladkevich, Sergey
AU - Gun, Jenny
AU - Bharathi, Subramanian
AU - Lev, Ovadia
AU - Prikhodchenko, Petr V.
PY - 2011
DA - 2011/11/01
PB - Elsevier
SP - 24-29
IS - 1
VL - 378
SN - 0020-1693
SN - 1873-3255
ER -
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BibTex (up to 50 authors)
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@article{2011_Mikhaylov,
author = {Alexey Mikhaylov and E A Melnik and Andrei V. Churakov and Vladimir M. Novotortsev and Judith A. Howard and Sergey Sladkevich and Jenny Gun and Subramanian Bharathi and Ovadia Lev and Petr V. Prikhodchenko},
title = {Synthesis, crystal structure and characterization of alkali metal hydroxoantimonates},
journal = {Inorganica Chimica Acta},
year = {2011},
volume = {378},
publisher = {Elsevier},
month = {nov},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0020169311006499},
number = {1},
pages = {24--29},
doi = {10.1016/j.ica.2011.08.007}
}
Cite this
MLA
Copy
Mikhaylov, Alexey, et al. “Synthesis, crystal structure and characterization of alkali metal hydroxoantimonates.” Inorganica Chimica Acta, vol. 378, no. 1, Nov. 2011, pp. 24-29. https://linkinghub.elsevier.com/retrieve/pii/S0020169311006499.