Tetranuclear LnIII2 MnII2 cymantrenecarboxylates. Synthesis, structure, thermolysis and magnetic properties
Publication type: Journal Article
Publication date: 2014-07-01
scimago Q3
wos Q2
SJR: 0.393
CiteScore: 5.5
Impact factor: 3.2
ISSN: 00201693, 18733255
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Abstract New organometallic 3d–4f-heterometallic carboxylates [LnIII2MnII2(μ3-OH)2(μ-O,η2-O2CCym)2(μ2-O2CCym)6(THF)4] (Ln = Dy, Ho; Cym = (η5-C5H4)Mn(CO)3) having “defective dicubane” structure were synthesized by means of partial destructive photolysis of the cymantrenecarboxylate anion in the presence of Ln3+, O2 and H2O. The magnetic susceptibilities (dc and ac) for the complexes were measured. Magnetic properties of Dy complex are indicative of its single molecule magnet behavior, complex of Ho displays slow relaxation of the magnetization at liquid helium temperature. Thermolysis of the complexes was studied by means of TG and DSC.
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14
Total citations:
14
Citations from 2024:
0
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Citations in journal:
3
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Koroteev P. S. et al. Tetranuclear LnIII2MnII2 cymantrenecarboxylates. Synthesis, structure, thermolysis and magnetic properties // Inorganica Chimica Acta. 2014. Vol. 418. pp. 157-162.
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Koroteev P. S., Efimov N. N., Ilyukhin A. B., Dobrokhotova Z. V., Novotortsev V. M. Tetranuclear LnIII2MnII2 cymantrenecarboxylates. Synthesis, structure, thermolysis and magnetic properties // Inorganica Chimica Acta. 2014. Vol. 418. pp. 157-162.
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TY - JOUR
DO - 10.1016/j.ica.2014.04.029
UR - https://linkinghub.elsevier.com/retrieve/pii/S0020169314002345
TI - Tetranuclear LnIII2MnII2 cymantrenecarboxylates. Synthesis, structure, thermolysis and magnetic properties
T2 - Inorganica Chimica Acta
AU - Koroteev, Pavel S
AU - Efimov, Nikolay N.
AU - Ilyukhin, Andrey B.
AU - Dobrokhotova, Zhanna V
AU - Novotortsev, Vladimir M.
PY - 2014
DA - 2014/07/01
PB - Elsevier
SP - 157-162
VL - 418
SN - 0020-1693
SN - 1873-3255
ER -
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@article{2014_Koroteev,
author = {Pavel S Koroteev and Nikolay N. Efimov and Andrey B. Ilyukhin and Zhanna V Dobrokhotova and Vladimir M. Novotortsev},
title = {Tetranuclear LnIII2MnII2 cymantrenecarboxylates. Synthesis, structure, thermolysis and magnetic properties},
journal = {Inorganica Chimica Acta},
year = {2014},
volume = {418},
publisher = {Elsevier},
month = {jul},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0020169314002345},
pages = {157--162},
doi = {10.1016/j.ica.2014.04.029}
}
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