International Journal of Biological Macromolecules, volume 47, issue 4, pages 578-581

Synthesis and characterization of diethoxy phosphoryl chitosan

Publication typeJournal Article
Publication date2010-11-01
Quartile SCImago
Q1
Quartile WOS
Q1
Impact factor8.2
ISSN01418130, 18790003
Biochemistry
Molecular Biology
General Medicine
Structural Biology
Abstract
A novel diethoxy phosphoryl chitosan was successfully synthesized via Atherton-Todd reaction of chitosan with diethyl phosphite, and the characterization was carried out by FT IR, NMR, ICP, XRD, TG and SEM, respectively. The FT IR, (13)C NMR and (31)P NMR results showed that diethoxy phosphoryl group was grafted onto the amino group of chitosan. XRD indicated that the incorporation of diethoxy phosphoryl group into chitosan increased the crystalline structure of the polymer. TG demonstrated that diethoxy phosphoryl chitosan was more thermal stable than chitosan. This simple and efficient synthetic method provides a new approach to the preparation of N-phosphoryl chitosan derivatives. And this new derivative of chitosan will open new perspectives as bio-functional material.

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GOST |
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GOST Copy
Ma L. et al. Synthesis and characterization of diethoxy phosphoryl chitosan // International Journal of Biological Macromolecules. 2010. Vol. 47. No. 4. pp. 578-581.
GOST all authors (up to 50) Copy
Ma L., Li G., Li L., Liu P. Synthesis and characterization of diethoxy phosphoryl chitosan // International Journal of Biological Macromolecules. 2010. Vol. 47. No. 4. pp. 578-581.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1016/j.ijbiomac.2010.06.014
UR - https://doi.org/10.1016/j.ijbiomac.2010.06.014
TI - Synthesis and characterization of diethoxy phosphoryl chitosan
T2 - International Journal of Biological Macromolecules
AU - Ma, Li
AU - Li, Guanghua
AU - Li, Limin
AU - Liu, Pu
PY - 2010
DA - 2010/11/01 00:00:00
PB - Elsevier
SP - 578-581
IS - 4
VL - 47
SN - 0141-8130
SN - 1879-0003
ER -
BibTex |
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BibTex Copy
@article{2010_Ma,
author = {Li Ma and Guanghua Li and Limin Li and Pu Liu},
title = {Synthesis and characterization of diethoxy phosphoryl chitosan},
journal = {International Journal of Biological Macromolecules},
year = {2010},
volume = {47},
publisher = {Elsevier},
month = {nov},
url = {https://doi.org/10.1016/j.ijbiomac.2010.06.014},
number = {4},
pages = {578--581},
doi = {10.1016/j.ijbiomac.2010.06.014}
}
MLA
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MLA Copy
Ma, Li, et al. “Synthesis and characterization of diethoxy phosphoryl chitosan.” International Journal of Biological Macromolecules, vol. 47, no. 4, Nov. 2010, pp. 578-581. https://doi.org/10.1016/j.ijbiomac.2010.06.014.
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