Facile synthesis of hierarchical nanocrystalline ZSM-5 zeolite under mild conditions and its catalytic performance
Youming Ni
1
,
Aiming Sun
1
,
Xiao-Ling Wu
1
,
Guoliang Hai
1
,
Jianglin Hu
1
,
Tao Li
2
,
Guang-xing Li
2
Publication type: Journal Article
Publication date: 2011-09-01
scimago Q1
wos Q1
SJR: 1.885
CiteScore: 18.5
Impact factor: 9.7
ISSN: 00219797, 10957103
PubMed ID:
21714969
Surfaces, Coatings and Films
Electronic, Optical and Magnetic Materials
Colloid and Surface Chemistry
Biomaterials
Abstract
Hierarchical nanocrystalline ZSM-5 zeolite (NZ5) was synthesized at 100 °C under atmospheric pressure using methylamine as a mineralizing agent. The crystallization process of NZ5 was characterized by dynamic light scattering (DLS), X-ray diffraction (XRD), and infrared spectroscopy (FTIR). The results of contrastive experiments showed that evaporation of the solvent promoted the aggregation of primary particles, and the addition of methylamine accelerated the crystallization process. The NZ5 aggregate consisted of 20 nm individual particles, as shown in scanning electron microscope (SEM). The lattice fringes in the transmission electron microscope (TEM) images and the XRD results indicated that individual particles of NZ5 were highly crystalline. N(2) adsorption-desorption isotherms showed that NZ5 had high BET surface areas with mesopores having a mean diameter of about 9 nm. NZ5 exhibited a long lifetime, a stable and high yield of liquid hydrocarbons, and a high anti-coking performance in methanol-to-hydrocarbons reaction. Catalytic testing and TGA results showed that the lifetime of NZ5 was about ten times longer than that of micro-sized ZSM-5 zeolite (MZ5), and the average coking rate with NZ5 was one fifth over that of MZ5.
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Ni Y. et al. Facile synthesis of hierarchical nanocrystalline ZSM-5 zeolite under mild conditions and its catalytic performance // Journal of Colloid and Interface Science. 2011. Vol. 361. No. 2. pp. 521-526.
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Ni Y., Sun A., Wu X., Hai G., Hu J., Li T., Li G. Facile synthesis of hierarchical nanocrystalline ZSM-5 zeolite under mild conditions and its catalytic performance // Journal of Colloid and Interface Science. 2011. Vol. 361. No. 2. pp. 521-526.
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TY - JOUR
DO - 10.1016/j.jcis.2011.06.020
UR - https://doi.org/10.1016/j.jcis.2011.06.020
TI - Facile synthesis of hierarchical nanocrystalline ZSM-5 zeolite under mild conditions and its catalytic performance
T2 - Journal of Colloid and Interface Science
AU - Ni, Youming
AU - Sun, Aiming
AU - Wu, Xiao-Ling
AU - Hai, Guoliang
AU - Hu, Jianglin
AU - Li, Tao
AU - Li, Guang-xing
PY - 2011
DA - 2011/09/01
PB - Elsevier
SP - 521-526
IS - 2
VL - 361
PMID - 21714969
SN - 0021-9797
SN - 1095-7103
ER -
Cite this
BibTex (up to 50 authors)
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@article{2011_Ni,
author = {Youming Ni and Aiming Sun and Xiao-Ling Wu and Guoliang Hai and Jianglin Hu and Tao Li and Guang-xing Li},
title = {Facile synthesis of hierarchical nanocrystalline ZSM-5 zeolite under mild conditions and its catalytic performance},
journal = {Journal of Colloid and Interface Science},
year = {2011},
volume = {361},
publisher = {Elsevier},
month = {sep},
url = {https://doi.org/10.1016/j.jcis.2011.06.020},
number = {2},
pages = {521--526},
doi = {10.1016/j.jcis.2011.06.020}
}
Cite this
MLA
Copy
Ni, Youming, et al. “Facile synthesis of hierarchical nanocrystalline ZSM-5 zeolite under mild conditions and its catalytic performance.” Journal of Colloid and Interface Science, vol. 361, no. 2, Sep. 2011, pp. 521-526. https://doi.org/10.1016/j.jcis.2011.06.020.