Journal of Fluorine Chemistry

, том 125 , издание 4 , страницы 573-577

Synthesis of enantiomerically pure α-ethyl, α-vinyl and α-ethynyl 3,3,3-trifluoro alaninates

M. Crucianelli ¹

Francesco De Angelis ¹

Francesco Lazzaro ¹

Luciana Malpezzi ²

A. Volonterio ²

M. Zanda ³

Скрыть аффилиации авторов Показать аффилиации авторов: 3 аффилиации

Dipartimento di Chimica, Ingegneria Chimica e Materiali, Università di L'Aquila, Via Vetoio, I-67010 Coppito, Italy |

Dipartimento di Chimica, Materiali ed Ingegneria Chimica “G. Natta” del Politecnico di Milano, Via Mancinelli, 7, I-20131 Milan, Italy |

C.N.R.—Istituto di Chimica del Riconoscimento Molecolare, sezione “A. Quilico”, via Mancinelli 7, I-20131 Milan, Italy |

Тип публикации: Journal Article

Дата публикации: 2004-04-19

Elsevier

Journal of Fluorine Chemistry

scimago Q3

wos Q3

БС2

SJR: 0.333

CiteScore: 3.7

Impact factor: 1.9

ISSN: 00221139, 18733328

DOI: 10.1016/j.jfluchem.2003.11.034

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Organic Chemistry

Biochemistry

Inorganic Chemistry

Physical and Theoretical Chemistry

Environmental Chemistry

Краткое описание

We describe the first synthesis of enantiomerically pure (S)-α-vinyl and (S)-α-ethynyl 3,3,3-trifluoro alanine (TF-Ala) ethyl esters, starting from the in situ generated sulfinimine (S)-2 as key fluorinated building-block. (S)-α-Ethyl TF-Ala-OEt has been prepared as well by this route.

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Crucianelli M. et al. Synthesis of enantiomerically pure α-ethyl, α-vinyl and α-ethynyl 3,3,3-trifluoro alaninates // Journal of Fluorine Chemistry. 2004. Vol. 125. No. 4. pp. 573-577.

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Crucianelli M., De Angelis F., Lazzaro F., Malpezzi L., Volonterio A., Zanda M. Synthesis of enantiomerically pure α-ethyl, α-vinyl and α-ethynyl 3,3,3-trifluoro alaninates // Journal of Fluorine Chemistry. 2004. Vol. 125. No. 4. pp. 573-577.

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TY - JOUR

DO - 10.1016/j.jfluchem.2003.11.034

UR - https://doi.org/10.1016/j.jfluchem.2003.11.034

TI - Synthesis of enantiomerically pure α-ethyl, α-vinyl and α-ethynyl 3,3,3-trifluoro alaninates

T2 - Journal of Fluorine Chemistry

AU - Crucianelli, M.

AU - De Angelis, Francesco

AU - Lazzaro, Francesco

AU - Malpezzi, Luciana

AU - Volonterio, A.

AU - Zanda, M.

PY - 2004

DA - 2004/04/19

PB - Elsevier

SP - 573-577

IS - 4

VL - 125

SN - 0022-1139

SN - 1873-3328

ER -

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@article{2004_Crucianelli,

author = {M. Crucianelli and Francesco De Angelis and Francesco Lazzaro and Luciana Malpezzi and A. Volonterio and M. Zanda},

title = {Synthesis of enantiomerically pure α-ethyl, α-vinyl and α-ethynyl 3,3,3-trifluoro alaninates},

journal = {Journal of Fluorine Chemistry},

year = {2004},

volume = {125},

publisher = {Elsevier},

month = {apr},

url = {https://doi.org/10.1016/j.jfluchem.2003.11.034},

number = {4},

pages = {573--577},

doi = {10.1016/j.jfluchem.2003.11.034}

}

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Crucianelli, M., et al. “Synthesis of enantiomerically pure α-ethyl, α-vinyl and α-ethynyl 3,3,3-trifluoro alaninates.” Journal of Fluorine Chemistry, vol. 125, no. 4, Apr. 2004, pp. 573-577. https://doi.org/10.1016/j.jfluchem.2003.11.034.