Journal of Luminescence, volume 146, pages 133-140

Structural, optical and crystal field analyses of undoped and Mn2+-doped ZnS nanoparticles synthesized via reverse micelle route

R M Krsmanović Whiffen ¹

Dragana Jovanovic ¹

Ž. Antić ¹

B Bartova ²

Dušan D Milivojević ¹

Miroslav Dramicanin ¹

Mikhail G. Brik ³

Hide authors affiliations Show authors affiliations: 3 affiliations

Vinča Institute of Nuclear Sciences, University of Belgrade, P.O. Box 522, Belgrade 11001, Serbia |

LSME&CIME, École Polytechnique Fédérale de Lausanne, Station 12, Lausanne CH-101, Switzerland |

Institute of Physics, University of Tartu, Riia 142, Tartu 51014, Estonia |

Publication type: Journal Article

Publication date: 2014-02-01

Elsevier

Journal: Journal of Luminescence

Quartile SCImago

Quartile WOS

Impact factor: 3.6

ISSN: 00222313

DOI: 10.1016/j.jlumin.2013.09.032

Copy DOI

General Chemistry

Biochemistry

Biophysics

Atomic and Molecular Physics, and Optics

Condensed Matter Physics

Abstract

Zinc sulfide, both as a bulk material and in nanocrystalline form, is a valuable luminescent material with important applications. Doped ZnS nanoparticles of around 5 nm are the material of choice for optoelectronic applications running in the UV region owing to their significant quantum size effect. This paper concerns detailed structural, spectroscopic and crystal field studies of ZnS nanoparticles, both pure and doped with Mn2+ ions, successfully synthesized at room temperature using a simple reverse micelle technique in the Triton X-100/cyclohexane medium. The resulting ZnS sphalerite phase smallsize nanoparticles (3-5 nm) have a much larger energy band gap ( similar to 4.7 eV) than that reported for the bulk ZnS (3.6 eV), thus confirming a pronounced quantum confinement effect. The electron paramagnetic resonance data provided evidence for the existence of two distinct environments for Mn2+ ions: the interior (core) and near the surface of the nanoparticles. The presence of an Mn2+-characteristic orange emission centered at 600 nm confirmed that our sample's were properly doped with Mn2+ ions, as the T-4(1)->(6)A(1) radiation transition could arise only on the basis of Mn2+ ions incorporated into the ZnS nanoparticles. To the best of our knowledge, our finding include the longest decay time component for the orange emission ever observed, timed at about 3.3 ms. The experimental excitation spectra were analyzed and the transitions assigned using the exchange charge model of theory of crystal field, which allowed to calculate the energy level scheme of the Mn2+ ions. The results presented in this paper provide us with detailed information about the ZnS sphalerite nanocrystals studied and can be readily applied to other similar systems. (C) 2013 Elsevier B.V. All rights reserved.

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Journal of Luminescence	Journal of Luminescence, 7, 11.29% Journal of Luminescence 7 publications, 11.29%
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Journal of Physical Chemistry C	Journal of Physical Chemistry C, 2, 3.23% Journal of Physical Chemistry C 2 publications, 3.23%
ACS applied materials & interfaces	ACS applied materials & interfaces, 2, 3.23% ACS applied materials & interfaces 2 publications, 3.23%
Physical Review B	Physical Review B, 1, 1.61% Physical Review B 1 publication, 1.61%
Materials	Materials, 1, 1.61% Materials 1 publication, 1.61%
Nanomaterials	Nanomaterials, 1, 1.61% Nanomaterials 1 publication, 1.61%
Journal of Radioanalytical and Nuclear Chemistry	Journal of Radioanalytical and Nuclear Chemistry, 1, 1.61% Journal of Radioanalytical and Nuclear Chemistry 1 publication, 1.61%
Journal of Materials Science	Journal of Materials Science, 1, 1.61% Journal of Materials Science 1 publication, 1.61%
Materials Chemistry and Physics	Materials Chemistry and Physics, 1, 1.61% Materials Chemistry and Physics 1 publication, 1.61%
Displays	Displays, 1, 1.61% Displays 1 publication, 1.61%
Journal of Physics and Chemistry of Solids	Journal of Physics and Chemistry of Solids, 1, 1.61% Journal of Physics and Chemistry of Solids 1 publication, 1.61%
IOP Conference Series: Materials Science and Engineering	IOP Conference Series: Materials Science and Engineering, 1, 1.61% IOP Conference Series: Materials Science and Engineering 1 publication, 1.61%
Materials Letters	Materials Letters, 1, 1.61% Materials Letters 1 publication, 1.61%
Applied Surface Science	Applied Surface Science, 1, 1.61% Applied Surface Science 1 publication, 1.61%
Thin Solid Films	Thin Solid Films, 1, 1.61% Thin Solid Films 1 publication, 1.61%
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Optik	Optik, 1, 1.61% Optik 1 publication, 1.61%
Materials Science in Semiconductor Processing	Materials Science in Semiconductor Processing, 1, 1.61% Materials Science in Semiconductor Processing 1 publication, 1.61%
Solid State Communications	Solid State Communications, 1, 1.61% Solid State Communications 1 publication, 1.61%
Ceramics International	Ceramics International, 1, 1.61% Ceramics International 1 publication, 1.61%
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Citations by publishers

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Elsevier	Elsevier, 25, 40.32% Elsevier 25 publications, 40.32%
Springer Nature	Springer Nature, 8, 12.9% Springer Nature 8 publications, 12.9%
American Chemical Society (ACS)	American Chemical Society (ACS), 7, 11.29% American Chemical Society (ACS) 7 publications, 11.29%
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The Electrochemical Society	The Electrochemical Society, 2, 3.23% The Electrochemical Society 2 publications, 3.23%
Multidisciplinary Digital Publishing Institute (MDPI)	Multidisciplinary Digital Publishing Institute (MDPI), 2, 3.23% Multidisciplinary Digital Publishing Institute (MDPI) 2 publications, 3.23%
Wiley	Wiley, 2, 3.23% Wiley 2 publications, 3.23%
Hindawi Limited	Hindawi Limited, 2, 3.23% Hindawi Limited 2 publications, 3.23%
American Physical Society (APS)	American Physical Society (APS), 1, 1.61% American Physical Society (APS) 1 publication, 1.61%
IOP Publishing	IOP Publishing, 1, 1.61% IOP Publishing 1 publication, 1.61%
American Institute of Physics (AIP)	American Institute of Physics (AIP), 1, 1.61% American Institute of Physics (AIP) 1 publication, 1.61%
Trans Tech Publications	Trans Tech Publications, 1, 1.61% Trans Tech Publications 1 publication, 1.61%
Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii	Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii, 1, 1.61% Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii 1 publication, 1.61%
	5 10 15 20 25

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Krsmanović Whiffen R. M. et al. Structural, optical and crystal field analyses of undoped and Mn2+-doped ZnS nanoparticles synthesized via reverse micelle route // Journal of Luminescence. 2014. Vol. 146. pp. 133-140.

GOST all authors (up to 50) Copy

Krsmanović Whiffen R. M., Jovanovic D., Antić Ž., Bartova B., Milivojević D. D., Dramicanin M., Brik M. G. Structural, optical and crystal field analyses of undoped and Mn2+-doped ZnS nanoparticles synthesized via reverse micelle route // Journal of Luminescence. 2014. Vol. 146. pp. 133-140.

RIS |

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RIS Copy

TY - JOUR

DO - 10.1016/j.jlumin.2013.09.032

UR - https://doi.org/10.1016/j.jlumin.2013.09.032

TI - Structural, optical and crystal field analyses of undoped and Mn2+-doped ZnS nanoparticles synthesized via reverse micelle route

T2 - Journal of Luminescence

AU - Krsmanović Whiffen, R M

AU - Jovanovic, Dragana

AU - Antić, Ž.

AU - Bartova, B

AU - Milivojević, Dušan D

AU - Dramicanin, Miroslav

AU - Brik, Mikhail G.

PY - 2014

DA - 2014/02/01 00:00:00

PB - Elsevier

SP - 133-140

VL - 146

SN - 0022-2313

ER -

BibTex

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BibTex Copy

@article{2014_Krsmanović Whiffen,

author = {R M Krsmanović Whiffen and Dragana Jovanovic and Ž. Antić and B Bartova and Dušan D Milivojević and Miroslav Dramicanin and Mikhail G. Brik},

title = {Structural, optical and crystal field analyses of undoped and Mn2+-doped ZnS nanoparticles synthesized via reverse micelle route},

journal = {Journal of Luminescence},

year = {2014},

volume = {146},

publisher = {Elsevier},

month = {feb},

url = {https://doi.org/10.1016/j.jlumin.2013.09.032},

pages = {133--140},

doi = {10.1016/j.jlumin.2013.09.032}

}

Found error?

Publisher

Elsevier

Journal

Journal of Luminescence

Quartile SCImago

Quartile WOS

Impact factor

3.6

ISSN

00222313 (Print)