Palladium(I) carbonyl carboxylate clusters cyclo-[Pd2 (μ-CO)2 (μ-OCOR)2 ]n (n = 2 or 3): Structure and reactivity
Tatiana A Stromnova
1
,
O.N. Shishilov
1
,
Mikhail V Dayneko
2
,
Ludmila G Kuzmina
1
,
Judith A. Howard
3
Publication type: Journal Article
Publication date: 2006-09-01
scimago Q3
wos Q2
SJR: 0.385
CiteScore: 4.1
Impact factor: 2.4
ISSN: 0022328X, 18728561
Materials Chemistry
Organic Chemistry
Biochemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
The interaction of palladium(+1) cluster Pd 4 (μ-CO) 4 (μ-OAc) 4 with saturated and unsaturated carboxylic acids was studied. It was found, that the substitution of acetates groups on others carboxylates leads to the clusters with different nuclearity. Palladium(+1) carbonyl carboxylate complexes of composition [Pd(μ-CO)(μ-OCOR)] n , where R = CF 3 , CCl 3 , CH 2 Cl, MeCH = CMe, Me, Pr i , Bu, Bu i , Bu tert , n -C 5 H 11 and n = 4 or 6 were synthesized. According to X-ray data all clusters possess cyclic planar metal cores with alternate pairs of μ-carbonyl and μ-carboxylate ligands. The presence of bulky alkyl fragments in the carboxylate ligand increases the nuclearity of the cluster compared to that of the starting palladium(+1) carbonyl acetate of composition Pd 4 (μ-CO) 4 (μ-OAc) 4 due, apparently, to steric hindrance.
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Stromnova T. A. et al. Palladium(I) carbonyl carboxylate clusters cyclo-[Pd2(μ-CO)2(μ-OCOR)2]n (n = 2 or 3): Structure and reactivity // Journal of Organometallic Chemistry. 2006. Vol. 691. No. 18. pp. 3730-3736.
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Stromnova T. A., Monakhov K. Y., Shishilov O., Dayneko M. V., Churakov A. V., Kuzmina L. G., Howard J. A. Palladium(I) carbonyl carboxylate clusters cyclo-[Pd2(μ-CO)2(μ-OCOR)2]n (n = 2 or 3): Structure and reactivity // Journal of Organometallic Chemistry. 2006. Vol. 691. No. 18. pp. 3730-3736.
Cite this
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TY - JOUR
DO - 10.1016/j.jorganchem.2006.03.033
UR - https://linkinghub.elsevier.com/retrieve/pii/S0022328X06002531
TI - Palladium(I) carbonyl carboxylate clusters cyclo-[Pd2(μ-CO)2(μ-OCOR)2]n (n = 2 or 3): Structure and reactivity
T2 - Journal of Organometallic Chemistry
AU - Stromnova, Tatiana A
AU - Monakhov, Kirill Yu.
AU - Shishilov, O.N.
AU - Dayneko, Mikhail V
AU - Churakov, Andrei V.
AU - Kuzmina, Ludmila G
AU - Howard, Judith A.
PY - 2006
DA - 2006/09/01
PB - Elsevier
SP - 3730-3736
IS - 18
VL - 691
SN - 0022-328X
SN - 1872-8561
ER -
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BibTex (up to 50 authors)
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@article{2006_Stromnova,
author = {Tatiana A Stromnova and Kirill Yu. Monakhov and O.N. Shishilov and Mikhail V Dayneko and Andrei V. Churakov and Ludmila G Kuzmina and Judith A. Howard},
title = {Palladium(I) carbonyl carboxylate clusters cyclo-[Pd2(μ-CO)2(μ-OCOR)2]n (n = 2 or 3): Structure and reactivity},
journal = {Journal of Organometallic Chemistry},
year = {2006},
volume = {691},
publisher = {Elsevier},
month = {sep},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0022328X06002531},
number = {18},
pages = {3730--3736},
doi = {10.1016/j.jorganchem.2006.03.033}
}
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MLA
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Stromnova, Tatiana A., et al. “Palladium(I) carbonyl carboxylate clusters cyclo-[Pd2(μ-CO)2(μ-OCOR)2]n (n = 2 or 3): Structure and reactivity.” Journal of Organometallic Chemistry, vol. 691, no. 18, Sep. 2006, pp. 3730-3736. https://linkinghub.elsevier.com/retrieve/pii/S0022328X06002531.