Novel sandwich complexes of zirconium [C9 H5 (SiMe3 )2 ](C5 Me4 R)ZrCl2 (R = CH3 , CH2 CH2 NMe2 ): Synthesis and reduction behavior
Sergey A Belov
1
,
Roman S. Kirsanov
1
,
Dmitrii P. Krut’ko
1
,
Dmitrii A. Lemenovskii
1
,
Judith A. Howard
3
Publication type: Journal Article
Publication date: 2008-05-01
scimago Q3
wos Q2
SJR: 0.385
CiteScore: 4.1
Impact factor: 2.4
ISSN: 0022328X, 18728561
Materials Chemistry
Organic Chemistry
Biochemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Abstract Novel half-sandwich [C 9 H 5 (SiMe 3 ) 2 ]ZrCl 3 ( 3 ) and sandwich [C 9 H 5 (SiMe 3 ) 2 ](C 5 Me 4 R)ZrCl 2 (R = CH 3 ( 1) , CH 2 CH 2 NMe 2 ( 2 )) complexes were prepared and characterized. The reduction of 2 by Mg in THF lead to (η 5 -C 9 H 5 (SiMe 3 ) 2 )[η 5 :η 2 ( C , N )-C 5 Me 4 CH 2 CH 2 N(Me)CH 2 ]ZrH ( 7 ). The structure of 7 was proved by NMR spectroscopy data. Hydrolysis of 2 resulted in the binuclear complex ([C 5 Me 4 CH 2 CH 2 NMe 2 ]ZrCl 2 ) 2 O ( 6 ). The crystal structures of 1 and 6 were established by X-ray diffraction analysis.
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Belov S. A. et al. Novel sandwich complexes of zirconium [C9H5(SiMe3)2](C5 Me4R)ZrCl2 (R = CH3, CH2CH2NMe2): Synthesis and reduction behavior // Journal of Organometallic Chemistry. 2008. Vol. 693. No. 10. pp. 1912-1918.
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Belov S. A., Kirsanov R. S., Krut’ko D. P., Lemenovskii D. A., Churakov A. V., Howard J. A. Novel sandwich complexes of zirconium [C9H5(SiMe3)2](C5 Me4R)ZrCl2 (R = CH3, CH2CH2NMe2): Synthesis and reduction behavior // Journal of Organometallic Chemistry. 2008. Vol. 693. No. 10. pp. 1912-1918.
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TY - JOUR
DO - 10.1016/j.jorganchem.2008.02.019
UR - https://linkinghub.elsevier.com/retrieve/pii/S0022328X08001381
TI - Novel sandwich complexes of zirconium [C9H5(SiMe3)2](C5 Me4R)ZrCl2 (R = CH3, CH2CH2NMe2): Synthesis and reduction behavior
T2 - Journal of Organometallic Chemistry
AU - Belov, Sergey A
AU - Kirsanov, Roman S.
AU - Krut’ko, Dmitrii P.
AU - Lemenovskii, Dmitrii A.
AU - Churakov, Andrei V.
AU - Howard, Judith A.
PY - 2008
DA - 2008/05/01
PB - Elsevier
SP - 1912-1918
IS - 10
VL - 693
SN - 0022-328X
SN - 1872-8561
ER -
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BibTex (up to 50 authors)
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@article{2008_Belov,
author = {Sergey A Belov and Roman S. Kirsanov and Dmitrii P. Krut’ko and Dmitrii A. Lemenovskii and Andrei V. Churakov and Judith A. Howard},
title = {Novel sandwich complexes of zirconium [C9H5(SiMe3)2](C5 Me4R)ZrCl2 (R = CH3, CH2CH2NMe2): Synthesis and reduction behavior},
journal = {Journal of Organometallic Chemistry},
year = {2008},
volume = {693},
publisher = {Elsevier},
month = {may},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0022328X08001381},
number = {10},
pages = {1912--1918},
doi = {10.1016/j.jorganchem.2008.02.019}
}
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MLA
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Belov, Sergey A., et al. “Novel sandwich complexes of zirconium [C9H5(SiMe3)2](C5 Me4R)ZrCl2 (R = CH3, CH2CH2NMe2): Synthesis and reduction behavior.” Journal of Organometallic Chemistry, vol. 693, no. 10, May. 2008, pp. 1912-1918. https://linkinghub.elsevier.com/retrieve/pii/S0022328X08001381.