Palladium nitrosyl carboxylate clusters: Synthesis and reactivity. X-ray structures of Pd4 (μ-CO)2 (μ-NO)(μ-RCO 2 )5 (R = iPr, iBu)
O.N. Shishilov
1
,
Tatiana A Stromnova
1
,
Inessa A Efimenko
1
,
Judith A. Howard
2
,
Natalia A Minaeva
1
Publication type: Journal Article
Publication date: 2011-05-01
scimago Q3
wos Q2
SJR: 0.385
CiteScore: 4.1
Impact factor: 2.4
ISSN: 0022328X, 18728561
Materials Chemistry
Organic Chemistry
Biochemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Abstract New palladium nitrosyl carboxylate complexes Pd8(CO)4−m(NO)m(NO2)4(RCO2)8 (m = 2, 4) were obtained by the treatment of palladium carbonyl carboxylates clusters cyclo-Pdn(μ-CO)n(μ-RCO2)n (n = 6) (1) with gaseous nitrogen monoxide. These complexes are the products of CO substitution in early described Pd8(CO)4(NO2)4(RCO2)8 clusters. By adding an excess of corresponding acid to reaction mixture Pd4(CO)2(NO)(RCO2)5 complexes were obtained, their structures were determined by X-ray diffraction analysis. These clusters are intermediate products of transformation of 6-nuclear initial clusters into various 8-nuclear complexes. This fact demonstrates that carboxylate ligands can be used as stabilizers for intermediate unstable polynuclear palladium compounds.
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Shishilov O. et al. Palladium nitrosyl carboxylate clusters: Synthesis and reactivity. X-ray structures of Pd4(μ-CO)2(μ-NO)(μ-RCO 2)5 (R = iPr, iBu) // Journal of Organometallic Chemistry. 2011. Vol. 696. No. 10. pp. 2023-2029.
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Shishilov O., Stromnova T. A., Efimenko I. A., Churakov A. V., Howard J. A., Minaeva N. A. Palladium nitrosyl carboxylate clusters: Synthesis and reactivity. X-ray structures of Pd4(μ-CO)2(μ-NO)(μ-RCO 2)5 (R = iPr, iBu) // Journal of Organometallic Chemistry. 2011. Vol. 696. No. 10. pp. 2023-2029.
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TY - JOUR
DO - 10.1016/j.jorganchem.2010.10.056
UR - https://linkinghub.elsevier.com/retrieve/pii/S0022328X10006819
TI - Palladium nitrosyl carboxylate clusters: Synthesis and reactivity. X-ray structures of Pd4(μ-CO)2(μ-NO)(μ-RCO 2)5 (R = iPr, iBu)
T2 - Journal of Organometallic Chemistry
AU - Shishilov, O.N.
AU - Stromnova, Tatiana A
AU - Efimenko, Inessa A
AU - Churakov, Andrei V.
AU - Howard, Judith A.
AU - Minaeva, Natalia A
PY - 2011
DA - 2011/05/01
PB - Elsevier
SP - 2023-2029
IS - 10
VL - 696
SN - 0022-328X
SN - 1872-8561
ER -
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BibTex (up to 50 authors)
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@article{2011_Shishilov,
author = {O.N. Shishilov and Tatiana A Stromnova and Inessa A Efimenko and Andrei V. Churakov and Judith A. Howard and Natalia A Minaeva},
title = {Palladium nitrosyl carboxylate clusters: Synthesis and reactivity. X-ray structures of Pd4(μ-CO)2(μ-NO)(μ-RCO 2)5 (R = iPr, iBu)},
journal = {Journal of Organometallic Chemistry},
year = {2011},
volume = {696},
publisher = {Elsevier},
month = {may},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0022328X10006819},
number = {10},
pages = {2023--2029},
doi = {10.1016/j.jorganchem.2010.10.056}
}
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MLA
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Shishilov, O.N., et al. “Palladium nitrosyl carboxylate clusters: Synthesis and reactivity. X-ray structures of Pd4(μ-CO)2(μ-NO)(μ-RCO 2)5 (R = iPr, iBu).” Journal of Organometallic Chemistry, vol. 696, no. 10, May. 2011, pp. 2023-2029. https://linkinghub.elsevier.com/retrieve/pii/S0022328X10006819.
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