Dynamic behavior of [(η5-C5 H4 CH 3 )Cr(CO)2 (μ-SBu)Pt(PPh3 )2 ] in solution
Publication type: Journal Article
Publication date: 2011-09-01
scimago Q3
wos Q2
SJR: 0.385
CiteScore: 4.1
Impact factor: 2.4
ISSN: 0022328X, 18728561
Materials Chemistry
Organic Chemistry
Biochemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Abstract The structure and dynamic behavior of complex [(η 5 -C 5 H 4 CH 3 )Cr(CO) 2 (μ-SBu)Pt(PPh 3 ) 2 ] in solution was studied by multinuclear ( 1 H, 13 C, 31 P) NMR spectroscopy including a phase-sensitive NOESY experiment. Increasing temperature causes rupture of the Cr–Pt bond in the three-membered ring of the complex and rotation of the S–Pt(PPh 3 ) 2 unit around the Cr–S bond line, followed by formation of a new Cr–Pt bond to close the ring. All activation parameters for this dynamic process have been determined.
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Sakharov S. G., Skabitsky I. V., Pasynskii A. A. Dynamic behavior of [(η5-C5H4CH 3)Cr(CO)2(μ-SBu)Pt(PPh3)2] in solution // Journal of Organometallic Chemistry. 2011. Vol. 696. No. 19. pp. 3062-3067.
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Sakharov S. G., Skabitsky I. V., Pasynskii A. A. Dynamic behavior of [(η5-C5H4CH 3)Cr(CO)2(μ-SBu)Pt(PPh3)2] in solution // Journal of Organometallic Chemistry. 2011. Vol. 696. No. 19. pp. 3062-3067.
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TY - JOUR
DO - 10.1016/j.jorganchem.2011.06.005
UR - https://doi.org/10.1016/j.jorganchem.2011.06.005
TI - Dynamic behavior of [(η5-C5H4CH 3)Cr(CO)2(μ-SBu)Pt(PPh3)2] in solution
T2 - Journal of Organometallic Chemistry
AU - Sakharov, Sergey G.
AU - Skabitsky, I. V.
AU - Pasynskii, A. A.
PY - 2011
DA - 2011/09/01
PB - Elsevier
SP - 3062-3067
IS - 19
VL - 696
SN - 0022-328X
SN - 1872-8561
ER -
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@article{2011_Sakharov,
author = {Sergey G. Sakharov and I. V. Skabitsky and A. A. Pasynskii},
title = {Dynamic behavior of [(η5-C5H4CH 3)Cr(CO)2(μ-SBu)Pt(PPh3)2] in solution},
journal = {Journal of Organometallic Chemistry},
year = {2011},
volume = {696},
publisher = {Elsevier},
month = {sep},
url = {https://doi.org/10.1016/j.jorganchem.2011.06.005},
number = {19},
pages = {3062--3067},
doi = {10.1016/j.jorganchem.2011.06.005}
}
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MLA
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Sakharov, Sergey G., et al. “Dynamic behavior of [(η5-C5H4CH 3)Cr(CO)2(μ-SBu)Pt(PPh3)2] in solution.” Journal of Organometallic Chemistry, vol. 696, no. 19, Sep. 2011, pp. 3062-3067. https://doi.org/10.1016/j.jorganchem.2011.06.005.