Palladium(II)–acetylacetonate complexes containing phosphine and diphosphine ligands and their catalytic activities in telomerization of 1,3-dienes with diethylamine
Publication type: Journal Article
Publication date: 2014-02-01
scimago Q3
wos Q2
SJR: 0.385
CiteScore: 4.1
Impact factor: 2.4
ISSN: 0022328X, 18728561
Materials Chemistry
Organic Chemistry
Biochemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
A series of novel [Pd(acac-O,O′)(PˆP)]BF4 and known complexes [Pd(acac-O,O′)(PR3)2]BF4 (PˆP = dppm (1), dppp (2), dppb (3), dppf (4); R = Ph (5), p-Tol (6), i-Pr (7); acac = 2,4-pentanedionato) were prepared by the reaction of [Pd(acac-O,O′)(MeCN)2]BF4 (1) with appropriate ligands. Complex 2 was characterized by single-crystal X-ray analysis. Models of the structure and IR wavenumbers assignments of the cations of 1–4 were obtained by DFT calculations. Synthesized complexes were tested as catalysts in the telomerization of isoprene and butadiene with diethylamine. In the case of telomerization of butadiene with diethylamine high catalyst activity (e.g. TOFav = 1940 h−1 and TON up to 17,480 for complex 5) was obtained.
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Suslov D. S. et al. Palladium(II)–acetylacetonate complexes containing phosphine and diphosphine ligands and their catalytic activities in telomerization of 1,3-dienes with diethylamine // Journal of Organometallic Chemistry. 2014. Vol. 752. pp. 37-43.
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Suslov D. S., Bykov M. V., Belova M. V., Abramov P. A., Tkach V. S. Palladium(II)–acetylacetonate complexes containing phosphine and diphosphine ligands and their catalytic activities in telomerization of 1,3-dienes with diethylamine // Journal of Organometallic Chemistry. 2014. Vol. 752. pp. 37-43.
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TY - JOUR
DO - 10.1016/j.jorganchem.2013.11.017
UR - https://doi.org/10.1016/j.jorganchem.2013.11.017
TI - Palladium(II)–acetylacetonate complexes containing phosphine and diphosphine ligands and their catalytic activities in telomerization of 1,3-dienes with diethylamine
T2 - Journal of Organometallic Chemistry
AU - Suslov, Dmitry S
AU - Bykov, Mikhail V
AU - Belova, Marina V
AU - Abramov, Pavel A
AU - Tkach, Vitaly S
PY - 2014
DA - 2014/02/01
PB - Elsevier
SP - 37-43
VL - 752
SN - 0022-328X
SN - 1872-8561
ER -
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@article{2014_Suslov,
author = {Dmitry S Suslov and Mikhail V Bykov and Marina V Belova and Pavel A Abramov and Vitaly S Tkach},
title = {Palladium(II)–acetylacetonate complexes containing phosphine and diphosphine ligands and their catalytic activities in telomerization of 1,3-dienes with diethylamine},
journal = {Journal of Organometallic Chemistry},
year = {2014},
volume = {752},
publisher = {Elsevier},
month = {feb},
url = {https://doi.org/10.1016/j.jorganchem.2013.11.017},
pages = {37--43},
doi = {10.1016/j.jorganchem.2013.11.017}
}
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