Coordination compounds of titanium (IV) and 2-hydroxymethyl-phenol derivatives: Their synthesis, structure and catalytic activity in ethylene and 1-hexene polymerization
Тип публикации: Journal Article
Дата публикации: 2015-11-01
scimago Q3
wos Q2
БС2
SJR: 0.385
CiteScore: 4.1
Impact factor: 2.4
ISSN: 0022328X, 18728561
Materials Chemistry
Organic Chemistry
Biochemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Краткое описание
A series of titanium complexes LTiCl2·(iPrOH)2 12-18 and heterobimetallic complex L2Ti·iPrOLi·THF 19 bearing saligenin-type [O,O]2- ligands 6-11 were synthesized in high yields from Cl2Ti(OiPr)2 or LiTi(OiPr)5. X-ray structure analyses for 15 and 19 revealed that these complexes adopt a distorted octahedron or distorted tetragonal pyramid geometry. When activated by binary activator {3Et2AlCl + Bu2Mg}, complexes 12-19 exhibited moderate to high activities toward ethylene and 1-hexene polymerization, giving high molecular weight polymers with broad molecular weight distributions. The results of this study show the unique ability of Li and Mg chlorides to improve the catalytic ability of post-metallocene pre-catalysts.
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Khrustalev V. N. et al. Coordination compounds of titanium (IV) and 2-hydroxymethyl-phenol derivatives: Their synthesis, structure and catalytic activity in ethylene and 1-hexene polymerization // Journal of Organometallic Chemistry. 2015. Vol. 797. pp. 159-164.
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Khrustalev V. N., Gagieva S. C., Solovev M. V., Kurmaev D. A., Kolosov N. A., Fedyanin I. V., Bulychev B. M. Coordination compounds of titanium (IV) and 2-hydroxymethyl-phenol derivatives: Their synthesis, structure and catalytic activity in ethylene and 1-hexene polymerization // Journal of Organometallic Chemistry. 2015. Vol. 797. pp. 159-164.
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TY - JOUR
DO - 10.1016/j.jorganchem.2015.08.017
UR - https://doi.org/10.1016/j.jorganchem.2015.08.017
TI - Coordination compounds of titanium (IV) and 2-hydroxymethyl-phenol derivatives: Their synthesis, structure and catalytic activity in ethylene and 1-hexene polymerization
T2 - Journal of Organometallic Chemistry
AU - Khrustalev, Victor N.
AU - Gagieva, Svetlana Ch
AU - Solovev, Michail V
AU - Kurmaev, Dmitrii A
AU - Kolosov, Nikolay A
AU - Fedyanin, Ivan V.
AU - Bulychev, B. M.
PY - 2015
DA - 2015/11/01
PB - Elsevier
SP - 159-164
VL - 797
SN - 0022-328X
SN - 1872-8561
ER -
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@article{2015_Khrustalev,
author = {Victor N. Khrustalev and Svetlana Ch Gagieva and Michail V Solovev and Dmitrii A Kurmaev and Nikolay A Kolosov and Ivan V. Fedyanin and B. M. Bulychev},
title = {Coordination compounds of titanium (IV) and 2-hydroxymethyl-phenol derivatives: Their synthesis, structure and catalytic activity in ethylene and 1-hexene polymerization},
journal = {Journal of Organometallic Chemistry},
year = {2015},
volume = {797},
publisher = {Elsevier},
month = {nov},
url = {https://doi.org/10.1016/j.jorganchem.2015.08.017},
pages = {159--164},
doi = {10.1016/j.jorganchem.2015.08.017}
}