Journal of Power Sources, volume 464, pages 228158

Halide doping effect on solvent-synthesized lithium argyrodites Li6PS5X (X= Cl, Br, I) superionic conductors

William A. Arnold ¹

William Arnold

Dominika A Buchberger ^{2, 3}

Yang Li

Yang Li ²

Mahendra Sunkara

Mahendra K. Sunkara ²

Thad Druffel

Thad Druffel ²

Hui Wang ¹

Hui Wang

Hide authors affiliations Show authors affiliations: 3 affiliations

Mechanical Engineering Department, University of Louisville, 332 Eastern Pkwy, Louisville, KY, 40292, USA |

Conn Center for Renewable Energy Research, University of Louisville, 216 Eastern Pkwy, Louisville, KY, 40208, USA |

Faculty of Chemistry, University of Warsaw, Pasteura 1, 02-093, Warsaw, Poland |

Publication type: Journal Article

Publication date: 2020-07-01

Elsevier

Journal: Journal of Power Sources

Quartile SCImago

Quartile WOS

Impact factor: 9.2

ISSN: 03787753

DOI: 10.1016/j.jpowsour.2020.228158

Copy DOI

Physical and Theoretical Chemistry

Electrical and Electronic Engineering

Energy Engineering and Power Technology

Renewable Energy, Sustainability and the Environment

Abstract

Halide-doped lithium argyrodites (Li6PS5X, X = Cl, Br or I) are one class of the most promising solid electrolyte candidates for solid-state Li batteries. However, similar to other superionic conductors, Li6PS5X argyrodites are mostly synthezied through high temperature solid-state reactions. Herein, we employ a solvent-based method to synthesize Li6PS5X argyrodites and study the halide doping (type and concentration) effect on their structure and properties. Using ethanol as the solvent medium, Li6PS5X and Li6PS5Cl·xLiCl (0 ≤ x ≤ 2) materials with precise composition control were achieved. The liquid-synthesized Li6PS5Cl showed the best ionic conductivity of 0.34 mS cm−1 at room temperature, followed by Li6PS5Br, with Li6PS5I being the worst. Interestingly, excess Cl content further increased the ionic conductivity of Li6PS5Cl·LiCl up to 0.53 mS cm−1 at room temperature and 5 mS cm−1 at 90 °C. In addition, the Li4Ti5O12/Li cell with Li6PS5Cl·LiCl solid electrolyte exhibited higher specific capacity (135 mAh g−1) than that of Li6PS5Cl-based cell (110 mAh g−1) at 0.2C. These results highlight a solvent-based synthesis method with precise composition control to study the halogen ion's effect on the structure and properties of lithium argyrodites, which would promote the development of lithium argyrodite solid electrolytes for applications in all-solid-state Li batteries.

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ACS applied materials & interfaces	ACS applied materials & interfaces, 3, 5.56% ACS applied materials & interfaces 3 publications, 5.56%
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ACS Energy Letters	ACS Energy Letters, 3, 5.56% ACS Energy Letters 3 publications, 5.56%
Journal of Power Sources	Journal of Power Sources, 2, 3.7% Journal of Power Sources 2 publications, 3.7%
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Nano Letters	Nano Letters, 1, 1.85% Nano Letters 1 publication, 1.85%
Advanced Sustainable Systems	Advanced Sustainable Systems, 1, 1.85% Advanced Sustainable Systems 1 publication, 1.85%
Functional Materials Letters	Functional Materials Letters, 1, 1.85% Functional Materials Letters 1 publication, 1.85%
Nanomaterials	Nanomaterials, 1, 1.85% Nanomaterials 1 publication, 1.85%
Nature Communications	Nature Communications, 1, 1.85% Nature Communications 1 publication, 1.85%
Materials Today Physics	Materials Today Physics, 1, 1.85% Materials Today Physics 1 publication, 1.85%
Progress in Energy	Progress in Energy, 1, 1.85% Progress in Energy 1 publication, 1.85%
Molecules	Molecules, 1, 1.85% Molecules 1 publication, 1.85%
Journal of Alloys and Compounds	Journal of Alloys and Compounds, 1, 1.85% Journal of Alloys and Compounds 1 publication, 1.85%
SSRN Electronic Journal	SSRN Electronic Journal, 1, 1.85% SSRN Electronic Journal 1 publication, 1.85%
Materials Today Communications	Materials Today Communications, 1, 1.85% Materials Today Communications 1 publication, 1.85%
Batteries & Supercaps	Batteries & Supercaps, 1, 1.85% Batteries & Supercaps 1 publication, 1.85%
Journal of the American Ceramic Society	Journal of the American Ceramic Society, 1, 1.85% Journal of the American Ceramic Society 1 publication, 1.85%
Small	Small, 1, 1.85% Small 1 publication, 1.85%
International Journal of Energy Research	International Journal of Energy Research, 1, 1.85% International Journal of Energy Research 1 publication, 1.85%
Chemistry of Materials	Chemistry of Materials, 1, 1.85% Chemistry of Materials 1 publication, 1.85%
Membranes	Membranes, 1, 1.85% Membranes 1 publication, 1.85%
Industrial & Engineering Chemistry Research	Industrial & Engineering Chemistry Research, 1, 1.85% Industrial & Engineering Chemistry Research 1 publication, 1.85%
Open Engineering	Open Engineering, 1, 1.85% Open Engineering 1 publication, 1.85%
Journal of Physical Chemistry C	Journal of Physical Chemistry C, 1, 1.85% Journal of Physical Chemistry C 1 publication, 1.85%
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	2 4 6 8 10 12 14
Elsevier	Elsevier, 14, 25.93% Elsevier 14 publications, 25.93%
American Chemical Society (ACS)	American Chemical Society (ACS), 12, 22.22% American Chemical Society (ACS) 12 publications, 22.22%
Wiley	Wiley, 6, 11.11% Wiley 6 publications, 11.11%
Springer Nature	Springer Nature, 5, 9.26% Springer Nature 5 publications, 9.26%
Royal Society of Chemistry (RSC)	Royal Society of Chemistry (RSC), 4, 7.41% Royal Society of Chemistry (RSC) 4 publications, 7.41%
Multidisciplinary Digital Publishing Institute (MDPI)	Multidisciplinary Digital Publishing Institute (MDPI), 3, 5.56% Multidisciplinary Digital Publishing Institute (MDPI) 3 publications, 5.56%
Walter de Gruyter	Walter de Gruyter, 3, 5.56% Walter de Gruyter 3 publications, 5.56%
World Scientific	World Scientific, 1, 1.85% World Scientific 1 publication, 1.85%
IOP Publishing	IOP Publishing, 1, 1.85% IOP Publishing 1 publication, 1.85%
Social Science Electronic Publishing	Social Science Electronic Publishing, 1, 1.85% Social Science Electronic Publishing 1 publication, 1.85%
The Electrochemical Society	The Electrochemical Society, 1, 1.85% The Electrochemical Society 1 publication, 1.85%
Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii	Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii, 1, 1.85% Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii 1 publication, 1.85%
	2 4 6 8 10 12 14

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Arnold W. et al. Halide doping effect on solvent-synthesized lithium argyrodites Li6PS5X (X= Cl, Br, I) superionic conductors // Journal of Power Sources. 2020. Vol. 464. p. 228158.

GOST all authors (up to 50) Copy

Arnold W., Arnold W. A., Buchberger D. A., Li Y., Li Y., Sunkara M., Sunkara M. K., Druffel T., Druffel T., Wang H., Wang H. Halide doping effect on solvent-synthesized lithium argyrodites Li6PS5X (X= Cl, Br, I) superionic conductors // Journal of Power Sources. 2020. Vol. 464. p. 228158.

RIS |

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RIS Copy

TY - JOUR

DO - 10.1016/j.jpowsour.2020.228158

UR - https://doi.org/10.1016/j.jpowsour.2020.228158

TI - Halide doping effect on solvent-synthesized lithium argyrodites Li6PS5X (X= Cl, Br, I) superionic conductors

T2 - Journal of Power Sources

AU - Arnold, William

AU - Buchberger, Dominika A

AU - Li, Yang

AU - Sunkara, Mahendra

AU - Druffel, Thad

AU - Wang, Hui

AU - Arnold, William A.

AU - Li, Yang

AU - Sunkara, Mahendra K.

AU - Druffel, Thad

AU - Wang, Hui

PY - 2020

DA - 2020/07/01 00:00:00

PB - Elsevier

SP - 228158

VL - 464

SN - 0378-7753

ER -

BibTex

Cite this

BibTex Copy

@article{2020_Arnold,

author = {William Arnold and Dominika A Buchberger and Yang Li and Mahendra Sunkara and Thad Druffel and Hui Wang and William A. Arnold and Yang Li and Mahendra K. Sunkara and Thad Druffel and Hui Wang},

title = {Halide doping effect on solvent-synthesized lithium argyrodites Li6PS5X (X= Cl, Br, I) superionic conductors},

journal = {Journal of Power Sources},

year = {2020},

volume = {464},

publisher = {Elsevier},

month = {jul},

url = {https://doi.org/10.1016/j.jpowsour.2020.228158},

pages = {228158},

doi = {10.1016/j.jpowsour.2020.228158}

}

Found error?

Publisher

Elsevier

Journal

Journal of Power Sources

Quartile SCImago

Quartile WOS

Impact factor

9.2

ISSN

03787753 (Print)