volume 178 issue 7 pages 2197-2204

The disordered cubic structure of Ca7Co3Ga 5O18

Publication typeJournal Article
Publication date2005-07-01
scimago Q2
wos Q1
SJR0.629
CiteScore6.8
Impact factor3.5
ISSN00224596, 1095726X
Materials Chemistry
Ceramics and Composites
Electronic, Optical and Magnetic Materials
Inorganic Chemistry
Physical and Theoretical Chemistry
Condensed Matter Physics
Abstract
The new mixed oxide having composition close to Ca{sub 7}Co{sub 3}Ga{sub 5}O{sub 18} was synthesized from CaCO{sub 3}, Co{sub 3}O{sub 4} and Ga{sub 2}O{sub 3} at 1150{sup o}C in air and studied by neutron and synchrotron X-ray powder diffraction, selected-area electron diffraction and high-resolution electron microscopy. The structure was refined, using time-of-flight (TOF) neutron powder diffraction data, in space group F432, with a=15.0487(4)A and Z=8, to R{sub F}=0.7%. It is considerably disordered, with four different tetrahedral sites randomly occupied by Co and Ga atoms at a ratio of 1:2. The tetrahedra form a disordered (Co{sub 1/3}Ga{sub 2/3})O{sub 2} 3D-framework inside which isolated CoO{sub 6} octahedra, surrounded by 8 Ca atoms, are located. The structure is related to the ordered structure of Ca{sub 14}Al{sub 10}Zn{sub 6}O{sub 35}. Electron diffraction patterns confirmed the symmetry and unit cell and revealed no diffuse scattering. High-resolution electron microscopy images showed the absence of extended structural defects.
Found 
Found 

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GOST Copy
Grins J. et al. The disordered cubic structure of Ca7Co3Ga 5O18 // Journal of Solid State Chemistry. 2005. Vol. 178. No. 7. pp. 2197-2204.
GOST all authors (up to 50) Copy
Grins J., Istomin S. Y., Svensson G., Attfield J. P., Antipov E. V. The disordered cubic structure of Ca7Co3Ga 5O18 // Journal of Solid State Chemistry. 2005. Vol. 178. No. 7. pp. 2197-2204.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1016/j.jssc.2005.04.029
UR - https://linkinghub.elsevier.com/retrieve/pii/S0022459605001532
TI - The disordered cubic structure of Ca7Co3Ga 5O18
T2 - Journal of Solid State Chemistry
AU - Grins, J.
AU - Istomin, Sergey Ya.
AU - Svensson, Gunnar
AU - Attfield, J. Paul
AU - Antipov, Evgeny V.
PY - 2005
DA - 2005/07/01
PB - Elsevier
SP - 2197-2204
IS - 7
VL - 178
SN - 0022-4596
SN - 1095-726X
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2005_Grins,
author = {J. Grins and Sergey Ya. Istomin and Gunnar Svensson and J. Paul Attfield and Evgeny V. Antipov},
title = {The disordered cubic structure of Ca7Co3Ga 5O18},
journal = {Journal of Solid State Chemistry},
year = {2005},
volume = {178},
publisher = {Elsevier},
month = {jul},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0022459605001532},
number = {7},
pages = {2197--2204},
doi = {10.1016/j.jssc.2005.04.029}
}
MLA
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MLA Copy
Grins, J., et al. “The disordered cubic structure of Ca7Co3Ga 5O18.” Journal of Solid State Chemistry, vol. 178, no. 7, Jul. 2005, pp. 2197-2204. https://linkinghub.elsevier.com/retrieve/pii/S0022459605001532.