Mg8 Rh4 B - A new type of boron stabilized Ti2 Ni structure
A.M. Alekseeva
1, 2
,
Artem M. Abakumov
1, 2, 3
,
Andreas Leithe-Jasper
4
,
W. Schnelle
4
,
Yurii Prots
4
,
P S Chizhov
1, 2
,
G. Van Tendeloo
5
,
2
Publication type: Journal Article
Publication date: 2006-09-01
scimago Q2
wos Q1
SJR: 0.629
CiteScore: 6.8
Impact factor: 3.5
ISSN: 00224596, 1095726X
Materials Chemistry
Ceramics and Composites
Electronic, Optical and Magnetic Materials
Inorganic Chemistry
Physical and Theoretical Chemistry
Condensed Matter Physics
Abstract
The new magnesium rhodium boron compound Mg 8 Rh 4 B has been synthesized by reaction of the metal powders with crystalline or amorphous boron or the RhB precursor. The crystal structure of Mg 8 Rh 4 B was solved using single-crystal X-ray diffraction data (space group Fd3m, a = 12.1711(4) A, Z = 8, 174 reflections, R F = 0.016). The crystal structure can be described as a filled Ti 2 Ni type where the interstitial sites 8b (1/2, 1/2, 1/2), located at the center of two nested Mg 4 Rh 4 tetrahedra, are occupied by boron atoms. Taking into account the absence of the Ti 2 Ni-type phase in the binary Mg-Rh system, the boron atoms can be considered as stabilizing this structural motif. From the bonding analysis with the electron localization function the crystal structure is described as covalently bonded [Rh 4 B] 3- anions, embedded in a cationic magnesium matrix.
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GOST
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Alekseeva A. et al. Mg8Rh4B - A new type of boron stabilized Ti2Ni structure // Journal of Solid State Chemistry. 2006. Vol. 179. No. 9. pp. 2751-2760.
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Alekseeva A., Abakumov A. M., Leithe-Jasper A., Schnelle W., Prots Y., Chizhov P. S., Van Tendeloo G., Antipov E. V., Grin Y. Mg8Rh4B - A new type of boron stabilized Ti2Ni structure // Journal of Solid State Chemistry. 2006. Vol. 179. No. 9. pp. 2751-2760.
Cite this
RIS
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TY - JOUR
DO - 10.1016/j.jssc.2005.11.029
UR - https://linkinghub.elsevier.com/retrieve/pii/S0022459605005712
TI - Mg8Rh4B - A new type of boron stabilized Ti2Ni structure
T2 - Journal of Solid State Chemistry
AU - Alekseeva, A.M.
AU - Abakumov, Artem M.
AU - Leithe-Jasper, Andreas
AU - Schnelle, W.
AU - Prots, Yurii
AU - Chizhov, P S
AU - Van Tendeloo, G.
AU - Antipov, Evgeny V.
AU - Grin, Yuri
PY - 2006
DA - 2006/09/01
PB - Elsevier
SP - 2751-2760
IS - 9
VL - 179
SN - 0022-4596
SN - 1095-726X
ER -
Cite this
BibTex (up to 50 authors)
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@article{2006_Alekseeva,
author = {A.M. Alekseeva and Artem M. Abakumov and Andreas Leithe-Jasper and W. Schnelle and Yurii Prots and P S Chizhov and G. Van Tendeloo and Evgeny V. Antipov and Yuri Grin},
title = {Mg8Rh4B - A new type of boron stabilized Ti2Ni structure},
journal = {Journal of Solid State Chemistry},
year = {2006},
volume = {179},
publisher = {Elsevier},
month = {sep},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0022459605005712},
number = {9},
pages = {2751--2760},
doi = {10.1016/j.jssc.2005.11.029}
}
Cite this
MLA
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Alekseeva, A.M., et al. “Mg8Rh4B - A new type of boron stabilized Ti2Ni structure.” Journal of Solid State Chemistry, vol. 179, no. 9, Sep. 2006, pp. 2751-2760. https://linkinghub.elsevier.com/retrieve/pii/S0022459605005712.