Open Access
Open access
Materials and Design, volume 183, pages 108143

Ti3C2Tx MXene characterization produced from SHS-ground Ti3AlC2

Bazhin Pavel
Shplis Nikolay 1
Polčak Josef
Stolin Alexander
Kuznetsov Denis
Shchetinin Igor
Bazhin P. M. 1, 2
Polčák J. 5, 6
Stolin Alexander 2
Kuznetsov D. V. 1
Publication typeJournal Article
Publication date2019-12-01
Quartile SCImago
Q1
Quartile WOS
Q1
Impact factor8.4
ISSN02641275, 18734197
General Materials Science
Mechanical Engineering
Mechanics of Materials
Abstract
MXenes are an emerging family of two-dimensional (2D) early transition metal carbides/nitrides that are produced by selective A-element chemical etching from 3D MAX phase counterpart. Herein we report a low-cost method combining self-propagation high-temperature synthesis (SHS) and grinding to produce Ti3AlC2 precursor and further its usage to obtain Ti3C2Tx MXene. The SHS-ground precursor requires the same etching conditions as pressure-less synthesized precursors to fully etch A-layer and convert the 3D structure into 2D state. The obtained MXenes are atomically-thin flakes with an average lateral size of 1–2 μm. The room temperature electrical resistivity of Ti3C2Tx based 11 μm-thick film ranges between 295 and 317 μΩ·cm. SHS combining with grinding in one step can be considered as a scalable method to MXene synthesis.

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Pazniak H. et al. Ti3C2Tx MXene characterization produced from SHS-ground Ti3AlC2 // Materials and Design. 2019. Vol. 183. p. 108143.
GOST all authors (up to 50) Copy
Pazniak H., Bazhin P., Shplis N., Komissarov A. S., Polčak J., Stolin A., Kuznetsov D., Shchetinin I., Kolesnikov E., Bazhin P. M., Shchetinin I., Komissarov A., Polčák J., Stolin A., Kuznetsov D. V. Ti3C2Tx MXene characterization produced from SHS-ground Ti3AlC2 // Materials and Design. 2019. Vol. 183. p. 108143.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1016/j.matdes.2019.108143
UR - https://doi.org/10.1016%2Fj.matdes.2019.108143
TI - Ti3C2Tx MXene characterization produced from SHS-ground Ti3AlC2
T2 - Materials and Design
AU - Pazniak, Hanna
AU - Bazhin, Pavel
AU - Shplis, Nikolay
AU - Komissarov, Alexey S.
AU - Polčak, Josef
AU - Stolin, Alexander
AU - Kuznetsov, Denis
AU - Shchetinin, Igor
AU - Kolesnikov, Evgeniy
AU - Bazhin, P. M.
AU - Shchetinin, Igor
AU - Komissarov, Alexander
AU - Polčák, J.
AU - Stolin, Alexander
AU - Kuznetsov, D. V.
PY - 2019
DA - 2019/12/01 00:00:00
PB - Elsevier
SP - 108143
VL - 183
SN - 0264-1275
SN - 1873-4197
ER -
BibTex
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BibTex Copy
@article{2019_Pazniak,
author = {Hanna Pazniak and Pavel Bazhin and Nikolay Shplis and Alexey S. Komissarov and Josef Polčak and Alexander Stolin and Denis Kuznetsov and Igor Shchetinin and Evgeniy Kolesnikov and P. M. Bazhin and Igor Shchetinin and Alexander Komissarov and J. Polčák and Alexander Stolin and D. V. Kuznetsov},
title = {Ti3C2Tx MXene characterization produced from SHS-ground Ti3AlC2},
journal = {Materials and Design},
year = {2019},
volume = {183},
publisher = {Elsevier},
month = {dec},
url = {https://doi.org/10.1016%2Fj.matdes.2019.108143},
pages = {108143},
doi = {10.1016/j.matdes.2019.108143}
}
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