Racemo-selective formation of ansa-zirconocene in the reaction of dimethylbis(5-phenyl-5,6-dihydroindeno[2,1-b]indol-6-yl)silane dilithium salt with ZrCl4 : X-ray and DFT argumentation for stereocontrol
Ilya E. Nifant'ev
1, 2
,
Alexander A Vinogradov
3
,
Konstantin A. Lyssenko
2, 4
,
Pavel V Ivchenko
1, 2
2
Publication type: Journal Article
Publication date: 2019-05-01
scimago Q3
wos Q3
SJR: 0.305
CiteScore: 3.0
Impact factor: 1.7
ISSN: 09599436, 1364551X
General Chemistry
Abstract
The reaction of bis[(5a,6,6a,10a,10b-η)-5-phenyl-5,6-dihydroindeno[2,1-b]indol-6-yl]dimethylsilane dilithium salt with ZrCl4 results in the formation of zirconium ansa-complex with >95% rac-selectivity, presumably due to specific crystal structure of the dilithium salt, which was established by X-ray diffraction.
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Nifant'ev I. E. et al. Racemo-selective formation of ansa-zirconocene in the reaction of dimethylbis(5-phenyl-5,6-dihydroindeno[2,1-b]indol-6-yl)silane dilithium salt with ZrCl4: X-ray and DFT argumentation for stereocontrol // Mendeleev Communications. 2019. Vol. 29. No. 3. pp. 266-268.
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Nifant'ev I. E., Vinogradov A. A., Minyaev M. E., Lyssenko K. A., Ivchenko P. V. Racemo-selective formation of ansa-zirconocene in the reaction of dimethylbis(5-phenyl-5,6-dihydroindeno[2,1-b]indol-6-yl)silane dilithium salt with ZrCl4: X-ray and DFT argumentation for stereocontrol // Mendeleev Communications. 2019. Vol. 29. No. 3. pp. 266-268.
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TY - JOUR
DO - 10.1016/j.mencom.2019.05.008
UR - https://linkinghub.elsevier.com/retrieve/pii/S0959943619301117
TI - Racemo-selective formation of ansa-zirconocene in the reaction of dimethylbis(5-phenyl-5,6-dihydroindeno[2,1-b]indol-6-yl)silane dilithium salt with ZrCl4: X-ray and DFT argumentation for stereocontrol
T2 - Mendeleev Communications
AU - Nifant'ev, Ilya E.
AU - Vinogradov, Alexander A
AU - Minyaev, Mikhail E.
AU - Lyssenko, Konstantin A.
AU - Ivchenko, Pavel V
PY - 2019
DA - 2019/05/01
PB - OOO Zhurnal "Mendeleevskie Soobshcheniya"
SP - 266-268
IS - 3
VL - 29
SN - 0959-9436
SN - 1364-551X
ER -
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@article{2019_Nifant'ev,
author = {Ilya E. Nifant'ev and Alexander A Vinogradov and Mikhail E. Minyaev and Konstantin A. Lyssenko and Pavel V Ivchenko},
title = {Racemo-selective formation of ansa-zirconocene in the reaction of dimethylbis(5-phenyl-5,6-dihydroindeno[2,1-b]indol-6-yl)silane dilithium salt with ZrCl4: X-ray and DFT argumentation for stereocontrol},
journal = {Mendeleev Communications},
year = {2019},
volume = {29},
publisher = {OOO Zhurnal "Mendeleevskie Soobshcheniya"},
month = {may},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0959943619301117},
number = {3},
pages = {266--268},
doi = {10.1016/j.mencom.2019.05.008}
}
Cite this
MLA
Copy
Nifant'ev, Ilya E., et al. “Racemo-selective formation of ansa-zirconocene in the reaction of dimethylbis(5-phenyl-5,6-dihydroindeno[2,1-b]indol-6-yl)silane dilithium salt with ZrCl4: X-ray and DFT argumentation for stereocontrol.” Mendeleev Communications, vol. 29, no. 3, May. 2019, pp. 266-268. https://linkinghub.elsevier.com/retrieve/pii/S0959943619301117.