Effective metal-free electrooxidative thiocyanation of anilines
Publication type: Journal Article
Publication date: 2022-01-01
scimago Q3
wos Q3
SJR: 0.305
CiteScore: 3.0
Impact factor: 1.7
ISSN: 09599436, 1364551X
General Chemistry
Abstract
An original anodic C–H thiocyanation of anilines with NH 4 SCN has been developed, allowing to obtain the products in 88–98% yields under potentiostatic diaphragm electrolysis on glassy carbon electrodes at E anode = 0.60 V and moderate consumption of electricity. The preliminary voltammetric analysis included the assessment of the changes in the thiocyanate ion curve after the addition of aniline, as well as the measurements of the potentials of the reagents and products, which gave insight into mechanisms of the process (formation of thiocyanate radical and thiocyanogen) and was necessary for its optimization.
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Khodonov V. M. et al. Effective metal-free electrooxidative thiocyanation of anilines // Mendeleev Communications. 2022. Vol. 32. No. 1. pp. 94-96.
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Khodonov V. M., Kudinova A. S., Kokorekin V. A., Petrosyan V. A., Egorov M. P. Effective metal-free electrooxidative thiocyanation of anilines // Mendeleev Communications. 2022. Vol. 32. No. 1. pp. 94-96.
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RIS
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TY - JOUR
DO - 10.1016/j.mencom.2022.01.030
UR - https://doi.org/10.1016/j.mencom.2022.01.030
TI - Effective metal-free electrooxidative thiocyanation of anilines
T2 - Mendeleev Communications
AU - Khodonov, V M
AU - Kudinova, A S
AU - Kokorekin, V A
AU - Petrosyan, V A
AU - Egorov, M P
PY - 2022
DA - 2022/01/01
PB - OOO Zhurnal "Mendeleevskie Soobshcheniya"
SP - 94-96
IS - 1
VL - 32
SN - 0959-9436
SN - 1364-551X
ER -
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BibTex (up to 50 authors)
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@article{2022_Khodonov,
author = {V M Khodonov and A S Kudinova and V A Kokorekin and V A Petrosyan and M P Egorov},
title = {Effective metal-free electrooxidative thiocyanation of anilines},
journal = {Mendeleev Communications},
year = {2022},
volume = {32},
publisher = {OOO Zhurnal "Mendeleevskie Soobshcheniya"},
month = {jan},
url = {https://doi.org/10.1016/j.mencom.2022.01.030},
number = {1},
pages = {94--96},
doi = {10.1016/j.mencom.2022.01.030}
}
Cite this
MLA
Copy
Khodonov, V. M., et al. “Effective metal-free electrooxidative thiocyanation of anilines.” Mendeleev Communications, vol. 32, no. 1, Jan. 2022, pp. 94-96. https://doi.org/10.1016/j.mencom.2022.01.030.
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