Mendeleev Communications
,  volume 32 ,  issue 4 ,  pages 567-569

The purity of SnCl4 as monitored by 35Cl nuclear quadrupole resonance

Publication type: Journal Article
Publication date: 2022-07-01
scimago Q3
wos Q3
SJR: 0.305
CiteScore: 3.0
Impact factor: 1.7
ISSN: 09599436, 1364551X
General Chemistry
Abstract
The nuclear quadrupole resonance (NQR) spectroscopy was used to control the comparative purity of three SnCl 4 samples subjected to successive stages of deep purification. The results showed that at 77 K the samples were identical in purity degree due to the ‘freezing’ of impurities into a separate fraction not affecting the perfection of the SnCl 4 crystal lattice. The results of relaxation measurements suggest that paramagnetic impurity atoms (Fe and Cr) contained in the samples in small amounts might be embedded into the crystal lattice causing extremely long spin–spin relaxation time.
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Kravchenko E. A. et al. The purity of SnCl4 as monitored by 35Cl nuclear quadrupole resonance // Mendeleev Communications. 2022. Vol. 32. No. 4. pp. 567-569.
GOST all authors (up to 50) Copy
Kravchenko E. A. The purity of SnCl4 as monitored by 35Cl nuclear quadrupole resonance // Mendeleev Communications. 2022. Vol. 32. No. 4. pp. 567-569.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1016/j.mencom.2022.07.044
UR - https://doi.org/10.1016/j.mencom.2022.07.044
TI - The purity of SnCl4 as monitored by 35Cl nuclear quadrupole resonance
T2 - Mendeleev Communications
AU - Kravchenko, Eleonora A
PY - 2022
DA - 2022/07/01
PB - OOO Zhurnal "Mendeleevskie Soobshcheniya"
SP - 567-569
IS - 4
VL - 32
SN - 0959-9436
SN - 1364-551X
ER -
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BibTex (up to 50 authors) Copy
@article{2022_Kravchenko,
author = {Eleonora A Kravchenko},
title = {The purity of SnCl4 as monitored by 35Cl nuclear quadrupole resonance},
journal = {Mendeleev Communications},
year = {2022},
volume = {32},
publisher = {OOO Zhurnal "Mendeleevskie Soobshcheniya"},
month = {jul},
url = {https://doi.org/10.1016/j.mencom.2022.07.044},
number = {4},
pages = {567--569},
doi = {10.1016/j.mencom.2022.07.044}
}
MLA
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MLA Copy
Kravchenko, Eleonora A., et al. “The purity of SnCl4 as monitored by 35Cl nuclear quadrupole resonance.” Mendeleev Communications, vol. 32, no. 4, Jul. 2022, pp. 567-569. https://doi.org/10.1016/j.mencom.2022.07.044.