An expedient cyclization of polyfunctional (aryl)(pyrimidinyl)(pyranyl)methanes into spiro[furo[3,2-c]pyran-2,5’-pyrimidine] scaffold
M. N. Elinson
1
,
Varvara M Kalashnikova
1, 2
,
Publication type: Journal Article
Publication date: 2023-07-17
scimago Q3
wos Q3
SJR: 0.305
CiteScore: 3.0
Impact factor: 1.7
ISSN: 09599436, 1364551X
General Chemistry
Abstract
Spirocyclization of morpholinium 3-[(aryl)(1,3-dimethyl-2,4,6-trioxohexahydropyrimidin-5-yl)methyl]-6-methyl-2-oxo-2H-pyran-4-olate by the action of sodium acetate-N-bromosuccinimide system in ethanol at room temperature results in spiro[furo[3,2-c]pyran-2,5’-pyrimidine] derivatives in 92–98% yields, the protocol allowing to avoid column chromatography purification. This new highly efficient and facile procedure is a convenient way to substituted unsymmetrical spiro scaffold containing pyrimidine-2,4,6-trione and 2,3-dihydro-4H-furo[3,2-c]pyran-4-one fragments promising for biomedical applications.
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Elinson M. N. et al. An expedient cyclization of polyfunctional (aryl)(pyrimidinyl)(pyranyl)methanes into spiro[furo[3,2-c]pyran-2,5’-pyrimidine] scaffold // Mendeleev Communications. 2023. Vol. 33. No. 4. pp. 448-450.
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Elinson M. N., Vereshchagin A. N., Ryzhkova Y. E., Karpenko K. A., Kalashnikova V. M., Egorov M. P. An expedient cyclization of polyfunctional (aryl)(pyrimidinyl)(pyranyl)methanes into spiro[furo[3,2-c]pyran-2,5’-pyrimidine] scaffold // Mendeleev Communications. 2023. Vol. 33. No. 4. pp. 448-450.
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TY - JOUR
DO - 10.1016/j.mencom.2023.06.002
UR - https://doi.org/10.1016/j.mencom.2023.06.002
TI - An expedient cyclization of polyfunctional (aryl)(pyrimidinyl)(pyranyl)methanes into spiro[furo[3,2-c]pyran-2,5’-pyrimidine] scaffold
T2 - Mendeleev Communications
AU - Elinson, M. N.
AU - Vereshchagin, Anatoly N.
AU - Ryzhkova, Yuliya E.
AU - Karpenko, Kirill A
AU - Kalashnikova, Varvara M
AU - Egorov, M. P.
PY - 2023
DA - 2023/07/17
PB - OOO Zhurnal "Mendeleevskie Soobshcheniya"
SP - 448-450
IS - 4
VL - 33
SN - 0959-9436
SN - 1364-551X
ER -
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BibTex (up to 50 authors)
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@article{2023_Elinson,
author = {M. N. Elinson and Anatoly N. Vereshchagin and Yuliya E. Ryzhkova and Kirill A Karpenko and Varvara M Kalashnikova and M. P. Egorov},
title = {An expedient cyclization of polyfunctional (aryl)(pyrimidinyl)(pyranyl)methanes into spiro[furo[3,2-c]pyran-2,5’-pyrimidine] scaffold},
journal = {Mendeleev Communications},
year = {2023},
volume = {33},
publisher = {OOO Zhurnal "Mendeleevskie Soobshcheniya"},
month = {jul},
url = {https://doi.org/10.1016/j.mencom.2023.06.002},
number = {4},
pages = {448--450},
doi = {10.1016/j.mencom.2023.06.002}
}
Cite this
MLA
Copy
Elinson, M. N., et al. “An expedient cyclization of polyfunctional (aryl)(pyrimidinyl)(pyranyl)methanes into spiro[furo[3,2-c]pyran-2,5’-pyrimidine] scaffold.” Mendeleev Communications, vol. 33, no. 4, Jul. 2023, pp. 448-450. https://doi.org/10.1016/j.mencom.2023.06.002.